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It works! A no-brainer tek. Followed the proportions in the Loveall tek.- toast seeds (10 g) and grind- add sodium carbonate and spray until doughy, incubate for 1-2 hr- oven dry (material turns dark)- mix with acetone, warmed until boiling acetone for 10 min with some mixing- decant and re-pull with acetone (total 80 mL)- add-in dry magnesium sulfate to collected acetone fractions (about 10 g) with occasional mix for 2 hr and rest to decant- filter yellow liquid- Add MASA or FASA, clouds form- room temperature incubate and watch slightly brown crystals grow!Working from seeds and there is no need for defatting? Unbelievable! This easy with minimal amount of reagents? Dying to see analytical data. Once yield is finished will post images.
It works! A no-brainer tek. Followed the proportions in the Loveall tek.
- toast seeds (10 g) and grind
- add sodium carbonate and spray until doughy, incubate for 1-2 hr
- oven dry (material turns dark)
- mix with acetone, warmed until boiling acetone for 10 min with some mixing
- decant and re-pull with acetone (total 80 mL)
- add-in dry magnesium sulfate to collected acetone fractions (about 10 g) with occasional mix for 2 hr and rest to decant
- filter yellow liquid
- Add MASA or FASA, clouds form
- room temperature incubate and watch slightly brown crystals grow!
Working from seeds and there is no need for defatting? Unbelievable! This easy with minimal amount of reagents? Dying to see analytical data. Once yield is finished will post images.