ava69
Rising Star
A way to make tetrahydroharmine:
Long time chemist, this method works very reliably well with 75% yield, similar to the 75% yield in TIHKAL
Someone wanted me to post a method here without writing about the effects of the pure THH, but I believe the two go hand and hand, the more you can find out about her, the better imho. So I will also post the link which contains all the info I know about her. She (THH) is a feminine spirit.
She is the Queen of psychedelics imho, combines extremely well with all sorts of psychedelics to bring out there essence. But even by herself:
This pure THH at 300mg all by herself is extremely visual, she's an isomer of a hormone like substance made in the brain naturally. With eyes closed for several hours are seen endless teaching visions: slow and high speed motion movies of nature, architecture, culture, history, the future, way beyond LSD or mescaline visuals...very realistic, mind-blowing...and with open eyes, beauty is extreme (over the top) and there is spiritual euphoria & joy, similar to mescaline.
She is like the beta-carboline version of mescaline, few people have used her over 100mg. I have seen the receptorome chart for THH vs. mescaline. She not only blocks serotonin like mescaline, but agonizes all 3 adrenal receptors A1-A3 associated with beauty and aesthetic enhancement, just like mescaline. A researcher I know has called her the tryptamine of the beta-carboline world, and rightly so.
Note: THH is NOT an MAOI, she (feminine spirit) is a psychedelic SRI or serotonin reuptake inhibitor just like the following psychedelic serotonin reuptake inhibitors: mescaline, LSD, shrooms, ibogaine.
Make sure your THH is pure and not contaminated with unconverted harmaline (which is a RIMA/maoi). Dab some THH on a wet cue tip, rub on paper plate, hold under blacklight, if it glows blue you have THH, if any green glow, you have harmaline in it, keep in mind harmine also glows blue too though.
DMT does not block serotonin on it's own, which is why I recommend taking the DMT along with the THH, just like in actual true Ayahuasca, important teamwork...all the daily survival filters and barriers will then be lifted, infinite mind will manifest & all spiritual things such as beauty, love, patience, music, art will then be seen for what they are: divine and infinite.
She is in the same beta-carboline family as ibogaine. She is the 2nd highest alkaloid in Caapi.
She has a 10.5 hour half-life with peak at 5.25 hours.
Beauty enhancement is "over the top" when THH is included. Music enhancement is profound and Heavenly as well. She has a very deep head space & profound spiritual insights.
Actresses on TV will look like dazzling glowing super-colorful cartoon caricatures of themselves (just like with high dose cactus tea) only if you include the THH with your Ayahuasca, 1-acetaldehyde LSD, or LSD.
Music will sound bad-ass incredible (way beyond LSD enhancement) only if you include from 150mg to 300mg oral THH with your Ayahuasca or 1-acetaldehyde LSD or plain LSD. Take them both orally at the same time.
1-acetaldehyde LSD instructions "how to" post #284: Journal: 50 Sublingual | <span style="frontcolor:pink !Important ;">High Pobability of Braindamage by Creepy non tested Drugs (forced by scammer 69ron)</span> | DMT Ayahuasca journeys over a years time - Pharmahuasca - Welcome to the DMT-Nexus
The entry in TIHKAL for 300mg THH is completely wrong, where the unexperienced person compares it to the effects of 100mg harmaline. She is nothing at all like harmaline, and like 69ron once said about the person's comment in TIHKAL, he or she would not be able to tell their ass from their elbow. I agree, what complete nonsense. Dr. Shulgin wrote that he never got the chance to try THH, but wrote that more studies on it are "badly needed."
See post #12 with pics:
Homo Trypens (10.21.2021) recently posted that he had success using the method, even though he did not seperate the harmaline from the harmine, he used a full spectrum extract. So it appears the THH he created contained a mixture of THH + harmine, see post #285:
Someone's well written essential dmt guide which I have read twice now: The Essential DMT Guide - DMT Discussion - Welcome to the DMT-Nexus
--------------------------------------------------------------
Part 10: One way to make tetrahydroharmine
Once you get to the end of your rue extraction, where you put your rue hcl in water and precipitate the harmine from the harmaline, you want to slowly bring the ph of the water up to exactly 7.0 with drops of 10% ammonia (from hardware store, the industrial janitorial version)...at 7.0 only the harmine will fall out, collect over vacuum filter...then raise ph to 7.5 or 8.0 (your preference) and collect a small middle fraction, which you will want to set aside as it is a mix of some harmaline with some harmine...keep this fraction to add back in the future when you do another rue extract...now collect the 3rd fraction, which is the harmaline only at ph = 7.5 or 8.0 and above.
Details: I dissolve the rue hcl extract into water on a stir mantel, and as the stir mantel spins....add drops of 10% ammonia to precipitate only the harmine 1st, then a very small middle fraction (harmine + harmaline), then a final fraction which is only harmaline. I prefer using 10% ammonia from hardware store (janitorial). Super good PH meter: Apera Instruments ph20 ph meter.
Now once you have your harmaline freebase...
1) place 10.5 grams of harmaline in a 1 liter pyrex cup style glass
2) add 900ml vinegar
3) add 40g zinc dust (from pyrotechnic places) in the pyrex glass too, use 40g zinc dust per each 10.5 grams of harmaline. You will see tiny hydrogen bubbles rise to the surface.
5) place beaker solution on a magnetic stirrer with stir rod and spin entire solution slowly
6) spin for 1.5 hour, the solution will turn from green to a transparent like color after 1.5 hour, use end of cotton q tip to place in solution and dab on paper plate in front of blacklight, it will now glow blue when transition is done...
7) once done with spin, let the solution sit for 1 hour, most (99%) of the zinc dust will settle to bottom, then filter solution over a #101 9cm filter disc fitted to a vacuum flask with vacuum trap in series with your vacuum pump, this will give you a transparent golden color liquid, use this solution for next step.
Throw away the zinc dust you just collected on filter disc (be careful, don't throw zinc on top aluminum foil in garbage or it will smoke due to hydrogen loaded zinc, best to put used zinc in a baggie with water to keep it moist, keep away from aluminum).
The pump/vacuum filter flask & filter disc will remove 100% of any zinc dust. so in other words, filter pyrex beaker solution (takes out the zinc dust) over a #101 9cm filter disc fitted inside a vacuum filtration flask hooked up to a vacuum pump, with a small vacuum trap in series, in-between the filtration flask and the pump. A good pump is JB platinum DV-142N 5 CFM heavy duty vacuum pump.
Cool you are left with a 100% clear transparent with just a touch of golden very light yellow color with no zinc dust at all...now add (80ml of 10% janitorial ammonia per 2g of harmaline)...so this means add 400ml of the 10% ammonia to your solution...you will immediately see the thh crash out of solution as a white powder, place mason jar in fridge for 3 hours, the crystals will all be seen at bottom of mason jar.
9) you will collect 7.5 grams of pure white THH freebase on the filter disc sitting in your vacuum filtration flask once you pour fridge cold solution over a #101 9cm filter disc in your vacuumm pump, rinse THH with some cold water. put filter disc of thh in a pyrex tray, scrape off and dry under fan...pure white.
10) always this will happen: exactly 75% is the yield, as I don't know why this is so...but it's a great yield still. Even in TIHKAL, the yield was similar, right at 75% as well.
11) The more zinc you use, the faster the reaction progresses, so 35 to 40g zinc means the reaction is finished by 1.5 hour.
I've looked at the #101 filter after filtration, hardly anything at all on it, truly only 1% of the zinc dust remains to be filtered after sitting for 1 hour.
If you don't have a vacuum pump/filtration setup: Personally, I believe the cotton ball in a funnel to be one of the greatest inventions of all time--and think it would work just fine for filtering out the remaining 1% zinc dust, remember 99% of the zinc dust falls to the bottom already after sitting for 1 hour after the spin mantel is turned off. What you are filtering is actually the 1% of zinc dust from the very bottom after sitting that get's kicked up back into the solution as you are decanting it off.
p.s. I also saw an episode of "Ancient Aliens" in which they discovered remnants of zinc dust inside one of the chambers, and they believe the Egyptians were making hydrogen gas using zinc and vinegar, speculating that the great pyramid was some sort of power generating device.
12) This THH at 300mg is extremely visual, she's an isomer of a hormone like substance made in the brain naturally. With eyes closed for several hours are seen endless slow and high speed motion movies of nature, architecture, culture, history, the future, way beyond LSD or mescaline visuals...very realistic, mind-blowing...and with open eyes, beauty is extreme (over the top) and there is spiritual joy....this is the best psychedelic secret kept under wraps...because hardly anyone has used it over 100mg.
Combine 250mg THH orally (take 45 minutes before) with sublingual 60mg of DMT complexed to 470mg HPBCD, add 10 drops boiling water, mash on a spoon hard back and forth for 2 minutes using the end of another spoon, mash or knead it all hard together using your muscles, grab off spoon using bottom side of tongue (it will all adhere) and hold for 15 minutes along with 30mg harmine freebase at the same time...22 minutes in you will experience profound beauty with open eyes, heavy CEV visions of spinning geometrics, actual temples, and ancient architecture, never ending breathtaking immaculate visions...pupils very dilated, music sounds incredible. 90 minutes long. 300mg THH is where the visions really are seen well, if you are not used to it, there is some slight dizziness at this dosage for a short period of time, but none at 250mg. The DMT really adds to the visions as well & brightens/colorizes them, incredible combination, just like in Ayahuasca. You can re-dose more HPBCD DMT every 1.5 hour x two more times.
Pic1: One way to make tetrahydroharmine
Pic2: Dissolve your rue hcl extract into warm 115 degree F water so it all dissolves, drop in two high precision PH meters, start the spin mantel, and add drops of 10% hardware store ammonia until you reach ph=7 when the harmine only will fall out, ph 7.1 to ph 7.9 = small middle fraction of harmaline mixed with harmine, put away and save for a rainy day when doing another extraction to add back in, ph 8.0 and above = all the harmaline only.
Long time chemist, this method works very reliably well with 75% yield, similar to the 75% yield in TIHKAL
Someone wanted me to post a method here without writing about the effects of the pure THH, but I believe the two go hand and hand, the more you can find out about her, the better imho. So I will also post the link which contains all the info I know about her. She (THH) is a feminine spirit.
She is the Queen of psychedelics imho, combines extremely well with all sorts of psychedelics to bring out there essence. But even by herself:
This pure THH at 300mg all by herself is extremely visual, she's an isomer of a hormone like substance made in the brain naturally. With eyes closed for several hours are seen endless teaching visions: slow and high speed motion movies of nature, architecture, culture, history, the future, way beyond LSD or mescaline visuals...very realistic, mind-blowing...and with open eyes, beauty is extreme (over the top) and there is spiritual euphoria & joy, similar to mescaline.
She is like the beta-carboline version of mescaline, few people have used her over 100mg. I have seen the receptorome chart for THH vs. mescaline. She not only blocks serotonin like mescaline, but agonizes all 3 adrenal receptors A1-A3 associated with beauty and aesthetic enhancement, just like mescaline. A researcher I know has called her the tryptamine of the beta-carboline world, and rightly so.
Note: THH is NOT an MAOI, she (feminine spirit) is a psychedelic SRI or serotonin reuptake inhibitor just like the following psychedelic serotonin reuptake inhibitors: mescaline, LSD, shrooms, ibogaine.
Make sure your THH is pure and not contaminated with unconverted harmaline (which is a RIMA/maoi). Dab some THH on a wet cue tip, rub on paper plate, hold under blacklight, if it glows blue you have THH, if any green glow, you have harmaline in it, keep in mind harmine also glows blue too though.
DMT does not block serotonin on it's own, which is why I recommend taking the DMT along with the THH, just like in actual true Ayahuasca, important teamwork...all the daily survival filters and barriers will then be lifted, infinite mind will manifest & all spiritual things such as beauty, love, patience, music, art will then be seen for what they are: divine and infinite.
She is in the same beta-carboline family as ibogaine. She is the 2nd highest alkaloid in Caapi.
She has a 10.5 hour half-life with peak at 5.25 hours.
Beauty enhancement is "over the top" when THH is included. Music enhancement is profound and Heavenly as well. She has a very deep head space & profound spiritual insights.
Actresses on TV will look like dazzling glowing super-colorful cartoon caricatures of themselves (just like with high dose cactus tea) only if you include the THH with your Ayahuasca, 1-acetaldehyde LSD, or LSD.
Music will sound bad-ass incredible (way beyond LSD enhancement) only if you include from 150mg to 300mg oral THH with your Ayahuasca or 1-acetaldehyde LSD or plain LSD. Take them both orally at the same time.
1-acetaldehyde LSD instructions "how to" post #284: Journal: 50 Sublingual | <span style="frontcolor:pink !Important ;">High Pobability of Braindamage by Creepy non tested Drugs (forced by scammer 69ron)</span> | DMT Ayahuasca journeys over a years time - Pharmahuasca - Welcome to the DMT-Nexus
The entry in TIHKAL for 300mg THH is completely wrong, where the unexperienced person compares it to the effects of 100mg harmaline. She is nothing at all like harmaline, and like 69ron once said about the person's comment in TIHKAL, he or she would not be able to tell their ass from their elbow. I agree, what complete nonsense. Dr. Shulgin wrote that he never got the chance to try THH, but wrote that more studies on it are "badly needed."
See post #12 with pics:
Homo Trypens (10.21.2021) recently posted that he had success using the method, even though he did not seperate the harmaline from the harmine, he used a full spectrum extract. So it appears the THH he created contained a mixture of THH + harmine, see post #285:
Someone's well written essential dmt guide which I have read twice now: The Essential DMT Guide - DMT Discussion - Welcome to the DMT-Nexus
--------------------------------------------------------------
Part 10: One way to make tetrahydroharmine
Once you get to the end of your rue extraction, where you put your rue hcl in water and precipitate the harmine from the harmaline, you want to slowly bring the ph of the water up to exactly 7.0 with drops of 10% ammonia (from hardware store, the industrial janitorial version)...at 7.0 only the harmine will fall out, collect over vacuum filter...then raise ph to 7.5 or 8.0 (your preference) and collect a small middle fraction, which you will want to set aside as it is a mix of some harmaline with some harmine...keep this fraction to add back in the future when you do another rue extract...now collect the 3rd fraction, which is the harmaline only at ph = 7.5 or 8.0 and above.
Details: I dissolve the rue hcl extract into water on a stir mantel, and as the stir mantel spins....add drops of 10% ammonia to precipitate only the harmine 1st, then a very small middle fraction (harmine + harmaline), then a final fraction which is only harmaline. I prefer using 10% ammonia from hardware store (janitorial). Super good PH meter: Apera Instruments ph20 ph meter.
Now once you have your harmaline freebase...
1) place 10.5 grams of harmaline in a 1 liter pyrex cup style glass
2) add 900ml vinegar
3) add 40g zinc dust (from pyrotechnic places) in the pyrex glass too, use 40g zinc dust per each 10.5 grams of harmaline. You will see tiny hydrogen bubbles rise to the surface.
5) place beaker solution on a magnetic stirrer with stir rod and spin entire solution slowly
6) spin for 1.5 hour, the solution will turn from green to a transparent like color after 1.5 hour, use end of cotton q tip to place in solution and dab on paper plate in front of blacklight, it will now glow blue when transition is done...
7) once done with spin, let the solution sit for 1 hour, most (99%) of the zinc dust will settle to bottom, then filter solution over a #101 9cm filter disc fitted to a vacuum flask with vacuum trap in series with your vacuum pump, this will give you a transparent golden color liquid, use this solution for next step.
Throw away the zinc dust you just collected on filter disc (be careful, don't throw zinc on top aluminum foil in garbage or it will smoke due to hydrogen loaded zinc, best to put used zinc in a baggie with water to keep it moist, keep away from aluminum).
The pump/vacuum filter flask & filter disc will remove 100% of any zinc dust. so in other words, filter pyrex beaker solution (takes out the zinc dust) over a #101 9cm filter disc fitted inside a vacuum filtration flask hooked up to a vacuum pump, with a small vacuum trap in series, in-between the filtration flask and the pump. A good pump is JB platinum DV-142N 5 CFM heavy duty vacuum pump.
Cool you are left with a 100% clear transparent with just a touch of golden very light yellow color with no zinc dust at all...now add (80ml of 10% janitorial ammonia per 2g of harmaline)...so this means add 400ml of the 10% ammonia to your solution...you will immediately see the thh crash out of solution as a white powder, place mason jar in fridge for 3 hours, the crystals will all be seen at bottom of mason jar.
9) you will collect 7.5 grams of pure white THH freebase on the filter disc sitting in your vacuum filtration flask once you pour fridge cold solution over a #101 9cm filter disc in your vacuumm pump, rinse THH with some cold water. put filter disc of thh in a pyrex tray, scrape off and dry under fan...pure white.
10) always this will happen: exactly 75% is the yield, as I don't know why this is so...but it's a great yield still. Even in TIHKAL, the yield was similar, right at 75% as well.
11) The more zinc you use, the faster the reaction progresses, so 35 to 40g zinc means the reaction is finished by 1.5 hour.
I've looked at the #101 filter after filtration, hardly anything at all on it, truly only 1% of the zinc dust remains to be filtered after sitting for 1 hour.
If you don't have a vacuum pump/filtration setup: Personally, I believe the cotton ball in a funnel to be one of the greatest inventions of all time--and think it would work just fine for filtering out the remaining 1% zinc dust, remember 99% of the zinc dust falls to the bottom already after sitting for 1 hour after the spin mantel is turned off. What you are filtering is actually the 1% of zinc dust from the very bottom after sitting that get's kicked up back into the solution as you are decanting it off.
p.s. I also saw an episode of "Ancient Aliens" in which they discovered remnants of zinc dust inside one of the chambers, and they believe the Egyptians were making hydrogen gas using zinc and vinegar, speculating that the great pyramid was some sort of power generating device.
12) This THH at 300mg is extremely visual, she's an isomer of a hormone like substance made in the brain naturally. With eyes closed for several hours are seen endless slow and high speed motion movies of nature, architecture, culture, history, the future, way beyond LSD or mescaline visuals...very realistic, mind-blowing...and with open eyes, beauty is extreme (over the top) and there is spiritual joy....this is the best psychedelic secret kept under wraps...because hardly anyone has used it over 100mg.
Combine 250mg THH orally (take 45 minutes before) with sublingual 60mg of DMT complexed to 470mg HPBCD, add 10 drops boiling water, mash on a spoon hard back and forth for 2 minutes using the end of another spoon, mash or knead it all hard together using your muscles, grab off spoon using bottom side of tongue (it will all adhere) and hold for 15 minutes along with 30mg harmine freebase at the same time...22 minutes in you will experience profound beauty with open eyes, heavy CEV visions of spinning geometrics, actual temples, and ancient architecture, never ending breathtaking immaculate visions...pupils very dilated, music sounds incredible. 90 minutes long. 300mg THH is where the visions really are seen well, if you are not used to it, there is some slight dizziness at this dosage for a short period of time, but none at 250mg. The DMT really adds to the visions as well & brightens/colorizes them, incredible combination, just like in Ayahuasca. You can re-dose more HPBCD DMT every 1.5 hour x two more times.
Pic1: One way to make tetrahydroharmine
Pic2: Dissolve your rue hcl extract into warm 115 degree F water so it all dissolves, drop in two high precision PH meters, start the spin mantel, and add drops of 10% hardware store ammonia until you reach ph=7 when the harmine only will fall out, ph 7.1 to ph 7.9 = small middle fraction of harmaline mixed with harmine, put away and save for a rainy day when doing another extraction to add back in, ph 8.0 and above = all the harmaline only.
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