BLAB 4b and 5b

[nukayo]

Hey guys
I use the BLAB tek to extract 100g of Mimosa.
I select FASW(4b and 5b)
I'm on 3a day on freezer and nothing cristalized...
Has a yellowish cloud dense accumulated in the bottom of the beaker, nothing more. The yellowish liquid through this too.

Can anyone help me?
Thanks!

 

[downwardsfromzero]

Looks OK to me. Might just be a bit damp in there.

 

[nukayo]

The last pull of water+dmt fumarate I put separated.
And the form of cristal are diferent, and the water is more clear!

Well. I think to put more NaOH and pull with limonene again...

 

[Entheogenerator]

I'm confused, you performed FASW, right? If so, you shouldn't be putting anything in the freezer... :?:

 

[downwardsfromzero]

I'm confused, you performed FASW, right? If so, you shouldn't be putting anything in the freezer... :?:

Well, a freezer is sort of a colder version of a fridge... sort of.

Yeah, I was a bit confused about that too.

The last pull of water+dmt fumarate I put separated.
And the form of cristal are diferent, and the water is more clear!

Just what are we looking at in the pictures? Water? Limonene?

Maybe you could describe in your own words the whole process you've been through up to this point?

Crystal forms can vary, sometimes seemingly for no apparent reason. When crystallising things, patience is the key. Give it another week.

 

[sjaman]

Well if you have fumaric acid, why dont you just go with Jorkest tek it almost the same as the BLAB tek without ipa you are following, but faster imho.

Evaporate the water and et voila dmt fumarate...

 

[nukayo]

On pics: Water + DMT Fumarate + Sodium Carbonate(to cristalize) (Water basified + "theoretically" freebase DMT)

With today is 5 days and nothing...
I put more NaOH and limonene, I will pull 4 times with 100mls of limonene, and do the FASW again