In theory if you did the freeze decant step then whatever goo you have should still be mostly pure mesc citrate. Just for whatever reason it seems not to crystallize in these cases :twisted: So that means if you used too much ethanol then you could simply also just evaporate everything to dryness and then it will not matter if you initially used too much.

But of course the ideal case would be to place it in the freezer and then decant what you have on top. Because of that it will be very easy to simply use very low amounts and heat to boiling, then mix very well with spoon or similar and then adding more if still not all is dissolved.

Maybe I would try like 10 ml for 50 g initial cacti powder.

I will probably need to do exactly the same again soon, as I failed to do the 69ron limonene tek properly and so I had to improvise by using CIELO on that emulsion, which nicely broke then emulsion then. So I will throw some citric acid on top soon and then if my luck continues will need to tackle that goo again :twisted: :twisted: