Dark brown oil solution is all whats left??? Help please

[J0rrit]

Hello,

I used this quantities: 500 ml water, 50 g mimosa, 50 g NaOH and 100 ml naphta ( x 3= 300 ml ) in total.

Now, when I put all of it in the freezer I get crystals, but they seem to be water crystals ( ice ) because when I filter them out of it they disappear. When I let all of the naphta evaporate instead of putting it in the freezer there's a dark brown substance left.... and that's all,, How can this be? Please help...

greets

 

[J0rrit]

Bump it up than... No one that has even a clu?

greets

 

[stevowitz]

your crystals arent strong enough to stand the room temp filter..

freeze it again and then when you've got crystals pour the naptha into another container.
let the empty, crystal-encrusted container air dry(I use a fan) and then scrape..

for some reason room-temp naptha will melt the stuff instantly, so you gotta seperate it before drying.

 

[J0rrit]

I did that. I even had the container ande filter in the freezer while filtering the whole stuff.... Didn't work either. If I just let the container dry ( let all the naphta evaporate ) it should just work wright? Now it looks as if there is just no dmt in the naptha....

 

[J0rrit]

Maybe it has to do with the way I separated the naptha from the rest of the substance... I had no pipet ( is that even english? ) or somethng like that and I just gutted all of the naphta out in a glass ( the substance was in a coca cola bottle ) and than separated the naphta from the glass using an injection needle ( without the actual needle ) to suck out the naptha. Or does it not matter wether the naphta shakes or ruffly moves and does the dmt just be in it?

greets

 

[gammagore]

The DMT should be in the naphta, I have no experience with the tek you used but sounds like you have bad bark dude.