WOW!!! you are the man, that the sort of response that Ive been waiting for. I got my Idea from smoking out of a bent test tube with a carb. At the top, the cool spots very pure dmt would recrystallize. I'm hoping the dmt will end up in the condenser, I was thinking a reflux might get it there but I've never done one and don't want to try it on good spice. It seems like this is something you'd need a two neck flask so you could put a thermometer into the naphtha, or a digital hotplate. I have neither, think I could pull it off with just a simple distillation setup with hotplate/stirrer?