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Does n-Oxide form in boiling solution?

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mombreast

mombreast

Rising Star
Hello there.
I appreciate if any of you can ansewer this question.

If I boil off DCM that contains DMT, does the DMT will become n-Oxide?

I read that heat tends to make n-oxide.
But if I am boiling, DMT can not get into contact with the air(oxgen).

And, what if I just heat the DCM just below the boiling poit of DCM?
Is this also not recommended?

I don't want to evap off DCM in my room, so I'll do it outside,
but don't want to let it sit there for a whole day,
beause any bird may dorp its shit to the beaker:d ...

so I want to finish the job as soon as possible.

Please help me, chemists.
Thanks for reading.
 
Thank you soulfood,
you seem to know a great deal about DMT.
I was under the impression tha heat in general is not good,
probably its a combo of heat+ fan that's wrong....

Thanks for the correction.
 
If heated in solution there is no problem, thats why we can boil down acidic extracts/make aya and have no problem and thats at the bp of water 100c not the bp of dcm ~40c. But if not in solutuion the DMT will boil away, and if exposed to a strong current of air (fan) for an extended amount of time dmt n-oxide will form.
 
mombreast: I think I read somewhere that DCM evaporates in an hour or so. Real quickly anyway so there is no need in my opinion to boil off DCM.
 
you must maximize the surface of your dmt if you want maximize the oxidation..so you could spread the powder in your owen or if you have some silicious sand you can wash it clean and than put it into a very concentrated solution al spread it and let it dry and oxidize in your oven,than recover with other clean solvent,this is the enhanced sand or lunar soil oxidizing tek!😉
 
Thank you all.
Swim recently finished zinc reduction and multiple recrystalizations to get fairly pure nnDMT.
However he seems to be highly sensitve to the chemical and doesn't feel prepared to the experience.
He used many tools from Bongs to GVG to crackpipes to electiric vaporizer to enhansed leaf to
copper scrubber and Volcano Vaporiser Liquid Pad but always coughs up really hard.

So... he tried freebased jimjam from Limo-FASA, and found that it's better for him.:d
As a consequence now he's interested in pure n-Oxide....

And thanks for the tip DiMiTrix, about the lunar soil oxidizing tek, but is oven a safe way to handle freebase DMT?
Or is there any established tek that can convert nnDMT to n-Oxide 100%?

I remember I read somewhere someone mentiond H2O2 for oxdization.
But where swim lives, only 3% H2O2 is availble.
 
mm never tried,swim thinks it could work if oven is no more than 100°C ,swim remembers of h2o2 too..
who know if swim could put the mhrb in oven for a while setting temp at low 90-100°c
 
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