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Shroombee, I got some results today also:- Simple tek- Salt slowly to ~neutral, clouds don't crash -> this is where I/we went into a loop of removing water, microwaving, etc. I think those things do help, and I got stuck on them for a bit, and drying the solvent may not work if citric acid is anhydrous, but there is simpler way (see next step).- Add more citric acid. Eventually pH paper becomes red and crashing occurs. Overtime solution becomes clear.- Filter and add more citric, no new clouds and no new crashing. I think this is the lazy man way of verifying that precipitation was completed in the previous step. The proper way would be to do an A/B on this and be extra sure.
Shroombee, I got some results today also:
- Simple tek
- Salt slowly to ~neutral, clouds don't crash -> this is where I/we went into a loop of removing water, microwaving, etc. I think those things do help, and I got stuck on them for a bit, and drying the solvent may not work if citric acid is anhydrous, but there is simpler way (see next step).
- Add more citric acid. Eventually pH paper becomes red and crashing occurs. Overtime solution becomes clear.
- Filter and add more citric, no new clouds and no new crashing. I think this is the lazy man way of verifying that precipitation was completed in the previous step. The proper way would be to do an A/B on this and be extra sure.