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It is definitely the chilled pull that makes a big difference for me. I think several factors will determine if we get crystalization or long needles:- Amount of plant material in the extract (less is better, chilled short pulls help here).- Amount of citric acid (too much and crystals will form to quickly to grow big, too little and complete crystallization may not happen)- Temperature: avoid quick temperature swings while xtals are forming- Shaking: With a lot of shaking xtals could be smaller and maybe grow fasterChilled solvent seems to help a lot with no major downsides. I also notice the xtals did not stick to the walls as when I do room temp pulls.What really convinces me is that when people have different cacti, or even whole cacti, chilled pulls should be a lot more robust to plant material variability. This is why I want the published TEK to use chilled ethyl acetate, so there are fewer potential issues in the future.
It is definitely the chilled pull that makes a big difference for me. I think several factors will determine if we get crystalization or long needles:
- Amount of plant material in the extract (less is better, chilled short pulls help here).
- Amount of citric acid (too much and crystals will form to quickly to grow big, too little and complete crystallization may not happen)
- Temperature: avoid quick temperature swings while xtals are forming
- Shaking: With a lot of shaking xtals could be smaller and maybe grow faster
Chilled solvent seems to help a lot with no major downsides. I also notice the xtals did not stick to the walls as when I do room temp pulls.
What really convinces me is that when people have different cacti, or even whole cacti, chilled pulls should be a lot more robust to plant material variability. This is why I want the published TEK to use chilled ethyl acetate, so there are fewer potential issues in the future.