Quick update: Added total of 18g Citric acid. The solvent cleared up completely (not color, just clarity). Very little precipitation a day later (a small amnt of gold-ish goo). After decanting there was some stickiness and something on sides. Dissolved in 30ml hot water as suggested to clean bottle sides, evaporating that now. Otherwise pretty much nothing except two blobs of the gold/brown goo in filter paper.

I guess either my source material is no longer much good or I got the pulls wrong somehow. But going over notes I cant see, but then the pulls kinda took all my attention and I only made notes afterwards.

Have more of the powder so I will try again. Bit disappointing but seeing the crystals above keeps me excited! I will start the harvest process with some pedros and bridges I have in the hope that that improves things!