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Update on the congealed sodium pastes with low yields (one using Na2CO3-0.7% and one using NaCl-0.6%).Yields recovered (back to 1%) by doing long warm extractions on the congealed paste. Product was more difficult to xtalize and crash (was sticking to the walls, had off colors, etc) and ended up having a slight tan color that did not wash off.I've started the MAS (microwave assisted saponification) + quick 0°F (using CaCl2 to avoid ice) extraction. I have a silicone coozy for the mason jar . Will report on this later this year, hoping for:- Near colorless extract with very little plant matter thanks to microwave breakdown/saponification and low temperature- Good yield (1%) - thanks to calcium making cacti in ethyl acetate sandy (large surface area)- Robust process to different starting cactus material giving large white crystals- Solvent reusable many times
Update on the congealed sodium pastes with low yields (one using Na2CO3-0.7% and one using NaCl-0.6%).
Yields recovered (back to 1%) by doing long warm extractions on the congealed paste. Product was more difficult to xtalize and crash (was sticking to the walls, had off colors, etc) and ended up having a slight tan color that did not wash off.
I've started the MAS (microwave assisted saponification) + quick 0°F (using CaCl2 to avoid ice) extraction. I have a silicone coozy for the mason jar . Will report on this later this year, hoping for:
- Near colorless extract with very little plant matter thanks to microwave breakdown/saponification and low temperature
- Good yield (1%) - thanks to calcium making cacti in ethyl acetate sandy (large surface area)
- Robust process to different starting cactus material giving large white crystals
- Solvent reusable many times