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That's wired your data is in post 679 for me and 680 for you I get what you mean by wanting to be lazy, that's the best. Perhaps we should update the L on CIELO from Leisurely to Lazily .The one and only point of boiling is for solvent reuse. The dark green color from the simple Tek worries me a little for reuse, but maybe it saturated and is perfectly OK? Using boiling water and re-loosening the paste right before pulling doesn't seem like a lot of added work, and the clearer solvent could be a lot easier to reuse and easier to see issues before xtalization (e.g. small particles or water layer).I'm seeing ~10% yield if doing 3 more pulls into a second jar. Barely worth it, but if I'm reusing solvent, why not? This is a good check everyone should do to make sure there first set of pulls into the first quart jar are good (to make sure the second jar doesn't have a lot of product).
That's wired your data is in post 679 for me and 680 for you
I get what you mean by wanting to be lazy, that's the best. Perhaps we should update the L on CIELO from Leisurely to Lazily .
The one and only point of boiling is for solvent reuse. The dark green color from the simple Tek worries me a little for reuse, but maybe it saturated and is perfectly OK? Using boiling water and re-loosening the paste right before pulling doesn't seem like a lot of added work, and the clearer solvent could be a lot easier to reuse and easier to see issues before xtalization (e.g. small particles or water layer).
I'm seeing ~10% yield if doing 3 more pulls into a second jar. Barely worth it, but if I'm reusing solvent, why not? This is a good check everyone should do to make sure there first set of pulls into the first quart jar are good (to make sure the second jar doesn't have a lot of product).