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Here’s weird, when i’m not logged in, the post is #679; when i’m logged in it’s #680.+1 on Leisurely -> Lazy, lol.You also worked the pulls more for the boiling treatment; it’s already quite a workout getting a good 1-min stir on quantities > than ~50g of material.Yes, if someone demonstrates a problem with the reused solvent from the std tek, i will certainly consider darkness of solvent a relevant consideration beyond exclusively crystal quality and quantity.Yes that is a good check, I would do it every time a new source of material is used, then compare yields of future runs (of same material) to save solvent and work. Additionally, before neutralizing solvent, a filtering should be done to capture crystals that developed after initial filtering.
Here’s weird, when i’m not logged in, the post is #679; when i’m logged in it’s #680.
+1 on Leisurely -> Lazy, lol.
You also worked the pulls more for the boiling treatment; it’s already quite a workout getting a good 1-min stir on quantities > than ~50g of material.
Yes, if someone demonstrates a problem with the reused solvent from the std tek, i will certainly consider darkness of solvent a relevant consideration beyond exclusively crystal quality and quantity.
Yes that is a good check, I would do it every time a new source of material is used, then compare yields of future runs (of same material) to save solvent and work. Additionally, before neutralizing solvent, a filtering should be done to capture crystals that developed after initial filtering.