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Finished my pulls, feeling pretty good about it. I got reverse osmosis water for this run, did 8 pulls with the recommended quantities, scaled for 25 grams. It was much easier without the lid in the way.Pulls 1-6 are combined, very dark green, clear, a few specks of dust. 7 and 8 much lighter green, looks like there's a tiny amount of stuff to decant.Decided to throw pulls 1-6 in my separatory funnel and leave it in there overnight for total confidence that there's no water. Of course, fancy thoughts like that anger the gods, and I forgot to close the stopcock, so I lost a few mL.
Finished my pulls, feeling pretty good about it. I got reverse osmosis water for this run, did 8 pulls with the recommended quantities, scaled for 25 grams. It was much easier without the lid in the way.
Pulls 1-6 are combined, very dark green, clear, a few specks of dust. 7 and 8 much lighter green, looks like there's a tiny amount of stuff to decant.
Decided to throw pulls 1-6 in my separatory funnel and leave it in there overnight for total confidence that there's no water. Of course, fancy thoughts like that anger the gods, and I forgot to close the stopcock, so I lost a few mL.