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Ok, i now undersrand this.Yep, only things i can think of are that solvent was so over diluted that the water was “bound” in the EA or not in freezer long enough. “Free” water in solvent should freeze into bottom ice layer and perhaps top ice shards.
Ok, i now undersrand this.
Yep, only things i can think of are that solvent was so over diluted that the water was “bound” in the EA or not in freezer long enough. “Free” water in solvent should freeze into bottom ice layer and perhaps top ice shards.
