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fastest extraction - Hyperspice Extraction Tek - By shoe

Migrated topic.

shoe

Rising Star
OG Pioneer
hyperspice extraction tek by shoe
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- A super fast variation of STB
extracting both red spice and DMT
freebase from mimosa root bark
(jurema)
---------------------------------

intro: the idea behind this tek was
to assess some of the problems with
the current STB teks and high volumes
of bark and evaporation process.
for impatient people like me.

AFAIK this is the FASTEST way from
bark to smoke with something of the
region of 1.5 hours maybe longer for your
first batch; yeild is on par with STB
+ Red spice extraction.

Many people (like myself) fall into
the trap of attempting to do 3Kg of
mimosa at once and simply can't handle
it in terms of volume, and then
end up hoarding their sludge because
they have too much and simply don't
get the yeilds they used to. etc.

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MAIN POINTS OF INTEREST
------------------------------------

This tek is quick and supplies about
4 - 5 hits VERY quickly, to get you
going, and when you want more, you can
simply do another bottle or six.

This tek is different in that its done
in small, small batches, exactly
how you would smoke your dmt anyway.

Additionally, you can just chuck the
depleted sludge, bottle and all,
right into the bin with no trouble.

don't hoard your gunk in hope of gaining
more DMT like i did! its pointless!!

also, don't leave your gunk sitting for
months, otherwise you'll loose alot
to DMT N-Oxide!!

use AS LITTLE naptha/xylene as possible
and you will be rewarded with quick
evaporation times!

There are NO massive cookdowns, NO a/b
extractions, no filtering, no fuss,
just 4 - 5 hits at a time,
and you can do it as many times as you
still have mimosa. This tek
because of the tiny batches, is also
very efficient. Your jurema also remains
in good condition and doesn't break down
while you are smoking your way through.

The fan heater I feel, is also a major
step forward.
------------------------------------
You will need:
------------------------------------
An electric fan heater
optional - extra fan
Glass baking dish
Turkey Baster
Small Pippette/Syringe
2L fizzy drinks bottle
Naptha (White spirit / Colemans Fuel)
Xylene (Paint thinner, xylol)
NaOH (sodium hydroxide, drain cleaner)
Funnel
Distilled water
Preground Mimosa hostillis rootbark (Jurema powder)

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for the super-pro's!
------------------------------------
fill 1/8th - 1/4 of a 2L plastic
drinks bottle with distilled water
excess naoh, and do 3 naptha pulls.
remove the soft inners of the lids!
this is quite important if you dont
enjoy smoking dissolved plastic!
only use about 1 cm - 1/2 inch of
solvent. Do them at 15mins, 15mins
and 3 hours. then do the xylene.
heat in a water bath, by boiling
the kettle and using a kitchen pot
or using the fan heater at a distance.

Chuck the sludge bottle in the bin,
and evaporate the extracts with a
fan heater on max and desk fan. Evap
the first pull while the third is
heating/sitting. Agitate frequently
but don't mess it up too much near
to when your going to seperate them.
recrystalize if you wish.

use your remaining mimosa for other
bottles.

------------------------------------
Lets go!
------------------------------------

1) Take a cup and a half or thereabouts of your preground mimosa hostillis, and using the funnel and perhaps a chopstick or similar, get it into the 2L plastic drinks bottle. At this point, remove the soft inner peice from
the inside of the lid. you must do this!! You want about 1/4 of the bottle filled with
jurema powder. one and a half cups should be fine. dont worry about using too little, you can't.

2) Mix it with the distilled water up to 3/4 - 80% of the volume of the bottle, just leave a small amount for the solvent. You want to use AS LITTLE SOLVENT AS HUMANLY POSSIBLE. Ideally, in a whole drinks bottle, you will have a centimeter (or about 1/2 an inch) of solvent at the top per extract. Think of it as: The more I add, The longer it will take. the worst part is, you don't necessarily get more either.

3) Using the funnel, add about 3 - 4 tablespoons of NaOH crystals. Be careful as this will warm the water. You want to add excess, so if you find your first pull doesn't go very well, add more NaOH. Im not sure if you can overbasify or not.

3) Boil the kettle and put the 2L bottle of black into a pot full of boiled water, to raise the temperature.

4) Put the lid on and shake the hell out of it. periodically shaking to try to get all the clumps of mimosa broken up. You were aiming for a sort of thin black liquid. Not too goopy, or it wont work.

5) fill up to the top of the bottle with naptha (on the first run), and squeeze the remaining air out of it and quickly screw the cap on. The less air in there, the less of an emulsion will form, but don't worry.

6) shake the hell out of it and let it sit for about 10 minutes, shaking every few minutes. This is to break the mimosa up and get the reaction going. The solvent should also float to the surface.

7) After ten minutes and its all shook up, turn it slowly end over end but don't shake it up, to allow the solvent to settle at the top. you can unscrew the lid here and use a syringe/dropper/tiny pipette to suck up the solvent and spray it back down to break up the bubbles of water-in-solvent (emulsion.)

8) after fifteen minutes or so, use the turkey baster at first, then the pipette/syringe to extract the top layer and deposit it into the glass tray. don't get any black in there.

9) repeat for the second extraction.

10) with the first and second extracts in the glass pan, get it in a well ventilated room with the electric fan on maximum and the other fan, if you've got one, also on maximum. Point them both at the pan, and let rip.

11) in as fast as 1 hour, but may take up to 3 hours, you will have your first batch of smokable extract. from my cup and a half of mimosa bark, I got about what looks to be between 1/4g and 3/4g. atleast 4 or 5 good hits anyway. Scrape it up and smoke it. You will be looking for clear or clear yellow blobs of liquid which won't evaporate. They are liquid DMT kept fluid or gum by the heat of the fan. as you take the dish away it will crystallize.

12) While your first extraction is evaporating (and I fnd this to be advantageous over freeze-precipitation, because you get ALL of the DMT from your extract, okay its not so pure, but you get far more mileage out of darker spice.) Get the third extraction in there, via the same steps as above, except let this one sit for as long as it takes to evaporate the first extracts. Leave the bottle, sealed, in the same room as the fan heater to keep it all nice and hot. (this helps extraction.)


Xylene pull:

After you have done 3 naptha extracts, you should do another 2 xylene ones. Again, use as little as possible and follow the instructions above. This will net you the lethally potent (BE VERY CAREFUL) and possibly extremely terrifying RED SPICE. You may need to recrystallize this stuff. See later.


Recrystallization:

Take your product (probably somekind of tan wax, yellow crystal or otherwise) and put it in a clean shotglass. Heat a small amount of naptha up, and dissolve the dmt freebase using as little as possible, with stirring. When its all gone, Cover the shotglass with tinfoil and shove it in the freezer. Don't put exposed naptha in your freezer or all of your food will taste of naptha FOREVER. and so will food you put in the freezer, too. Its disgusting, believe me!

After 2 - 4 hours you should have DMT crystals on the inside of the glass. Carefully decant the naptha and evaporate it down a little. then, do the same process on it once again. Alternatively, use it again for another recrystallization. dont use it more than twice, or it'll become to gunky. then, throw it away. you may also evaporate it down again, I guess, to yield low quality dmt gunk.


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Coming soon in version 2:
All of this, Plus how to net extra yeilds easilly
from DMT n-oxide conversion!

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Shoe
 
distiled water is just a good idea i always thought




also the bottles tey come in work great for mixing
they hold more then 2 liters too


you just gotta pour them into somthing else for the rollin
 
Distilled water is good to use because you KNOW there absolutely no impurities in it. I'm not sure in the UK but here in the US you can get it at any local grocery store. It won't rust metal so whatever reason you can think of, just don't say to drink it because i don't know of anyone that drinks distilled water. I dunno, the cashier doesn't even look at me, and it's only a doller for 1 gal.

I'm not sure if you would run into any problems being in the UK and all tho...
 
I actually just buy a huge bottle of something like evian (im sure they're international) or like general spring water.
You should be able to get it anywhere and everywhere.

the most important thing is that it doesn't have any chlorine in it, thats why I use it. So, your spice wont be broken down by
nasty free radicals, nor percipitated out by whatever else they add.

( have you ever repeatedly evaporated pan after pan of water and examined the residue?! OMG YUCK!!!)
 
Distilled water is, at least for me, very hard to find in the UK. You could try somewhere like Halfords but other than that I can't suggest anywhere. If you've got the kit it's easy enough to distill your own.
Spring water/mineral water isn't the same as distilled water, it'll taste better than tap water but I don't know that it'll be any better for an extraction as there will still be a lot of mineral content (in the ppm range). I didn't realise chlorine was an issue, don't think it's in the UK water though in any case.
 
Thanks guys - I managed to find distilled water labelled as de-ionised water in a small hardware shop that sells, shelves, nails, white spirit etc (sadly not Naptha but I ordered some of that online)

2 litres for £2

As I haven't got any Naptha yet is there any benefit of leaving the water, lye and Mimosa mixing together in a big glass jar for a couple of days? Or is it best to do a pull straight after 1 hour of it sitting?
 
I wouldn't advise more than a day, I think it converts gradually to dmt n-oxide. The NaOH part doesn't take long, its the solvent pulls and evap that take the longest.

But, hopefully when you've got everything this method should allow you some super fast extraction times. its definatley best to net 4 - 5 hits at a time, rather than
going for like 1039850 and it taking months...

Btw: also I feel the electric fan method is a MAJOR improvement over simply fanning. Get a thermometer on there and don't go above 60*C. TBH tho, even at
40 - 45 its pretty damn quick. If you use just a shotglass of naptha in total, it'll be done in an hour or two. Smoke up :D
 
ATTENZIONÉ!!!
---------------------------


Advanced research has shown that after 2 - 3 days of exposure the NaOH will dissolve the soft inner plastic part of the lid.

YOU MUST REMOVE THIS AT THE BEGINNING OF THE PROCESS. DO NOT SMOKE ANY DMT WHICH HAS GREY/WHITE CHUNKS OF WHAT LOOKS LIKE FAT
OR PLASTIC!

I have edited the tek accordingly.

Appart from this the tek works great, however I would reccomend a recrystalization as especially the xylene can be quite fatty.
Thanking you.
 
Here's a little question; I have Xylene well it's called Xylene Thinner and on the side of the can it says Xylene and a mixture of Isomers which wiki says are compounds with the same molecular formula, so is that the same? Not tried using it yet... cheers...
 
Well that one was recommended to SWIM and he has 5L of the stuff, been told it yealds good results but not tried it myself. As it's a white spirit the evap time is much longer compared to Coleman but it's much cheaper.

Still, def keep away from the Mistral Solvent Naptha because it's thick, orange, and water seems to suspend in it rather than sink to the bottom which is the expectation... will take another look though to confirm...
 
NOOOOOOOOOOOOOOOOOOOOOOOO Coleman's! theres an anti rust agent in there its green you can see it if you pour it in a glass and hold it to the light! also if you evap a little bit on a dish you'll see the bluish green oil. its very bad.... SWIM is speaking from experience! needless to say SWIM used it made very dirty DMT SWIM evaped it all and there was a green oil over top of his stuff SWIM blotted up with a paper towel and then scrapped it up. it was DMT but it was HARSH on the lungs and tasted especially bad. dont use it bad bad bad.

get VM&P naptha get your bums off your computer chair and check out the local hardware stores its in the paint section. absolutely NO Coleman's
 
Also, I wouldn't worry too much about evaporation times. What with the electric fan heater on the evapping, It powers through it in about < 45 minuites for a usual pull. Incredible that no one has thought of this before...

be careful though, I don't want anyone exploding themselves. Make sure the room is well ventilated.
 
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