I am doing a simple hermala FB extraction,skiping the doble filtration with ice and after that freebase the alcaloides.I go directly with the amonia for FB harmala after collection one purification is done redisolving the harmalas in vinager ,tilter the liquid to red dark transperent tee and one more time the amonia.I get for second time a very low yeld.And I don't think the provider's seeds are low quality.
Procedure
150 grams grinded seeds was boiled with some vinager three times for about 40 min each boil.Done at almost full speed boiling.Recolected all the liquid (very dense in color),and used a half of a bottle of amonia to change the color completly.
Weited 8h,filtered the harmalas.
Redisloved them in water/vinager and filtered the liquid.Transperent tee obtained
One more time used amonia until the liquid stop changing color.
Some gold harmala start to foll down.
Toatal ammount after filtering and drying -1 gr.
Where is the problem?
Procedure
150 grams grinded seeds was boiled with some vinager three times for about 40 min each boil.Done at almost full speed boiling.Recolected all the liquid (very dense in color),and used a half of a bottle of amonia to change the color completly.
Weited 8h,filtered the harmalas.
Redisloved them in water/vinager and filtered the liquid.Transperent tee obtained
One more time used amonia until the liquid stop changing color.
Some gold harmala start to foll down.
Toatal ammount after filtering and drying -1 gr.
Where is the problem?
