Help!! With stb powdered San Pedro tek

[Wavey Gravey]

I'm ready to begin a 100g stb mescaline extraction using powdered San Pedro.
I'm wondering if one should begin by adding basified water to the powdered s.p. or only enough distilled water to "rehydrate"and freeze 2-3 times to break the cell walls Or begin by adding basic distilled water Then freeze 2-3 times? Or is it a waste of time to freeze either way when using powdered s.p.??
Then let sit appx 24- 48 hr. Then adding xylene, shake let seperate 3-4 times then add citric acid & distilled water solution and evap after 4- 5 pulls??
Any and All input would be greatly appreciated!!
Thank You in advance to a Great Community!!
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[pete666]

try this
then salting/titration with HCl
then this
give me a shout if you need some more info

 

[Wavey Gravey]

Pete666
I am going to hold off on starting my experiment so as to give more thought to all you have given me to think about!!
Your Thorough Response is Greatly Appreciated!!
I may take you up on your most generous offer of more help/advice.
Thank You Sir!!
May All Your Experiments Be Emulsion Free & Pure!!
You are a Scholar and a Gentleman!!
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