Northerner
Rising Star
So as an experiment I ran almost half a kilo of phyllodes a/b-stb hybrid style, pulled with 2L of solvent and reduced to 350ml.
That 350ml of solvent I backsalted with 500ml of water.... The dmt actually flocculated when I based it.
Then I pulled again with another litre or so of fresh solvent and evapped it down a bit before sending to the freezer.
After I took it out from under the fan the solvent had chilled quite cool through endothermic reaction and in the bottom of the tray the DMT looked like a small amount of milk under the solvent.
Is this normal, (in the given parameters) or have I accidentally pulled some base somehow? This separated milk like substance concerns me as I haven't seen it before. Just highly concentrated DMT or base contamination?
That 350ml of solvent I backsalted with 500ml of water.... The dmt actually flocculated when I based it.
Then I pulled again with another litre or so of fresh solvent and evapped it down a bit before sending to the freezer.
After I took it out from under the fan the solvent had chilled quite cool through endothermic reaction and in the bottom of the tray the DMT looked like a small amount of milk under the solvent.
Is this normal, (in the given parameters) or have I accidentally pulled some base somehow? This separated milk like substance concerns me as I haven't seen it before. Just highly concentrated DMT or base contamination?