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Yes, I use glass for freeze precipitation - pint sized Mason jars typically.I think your first "failure" may not have been one. Maybe you didn't get a big yield and it all kind of disappeared in the filter. Did you try evaporating all of the remaining solvent to see if you wound up with some DMT?I have never done an ACRB extraction. And yet your problem is one I have heard described with MHRB. Maybe try turning your freezer up. That and/or leaving your jar in longer - and put it in the back right where the freezing air comes in. Also, BEFORE placing DMT containing naphtha in your freezer, evaporate off about 1/2 the total volume. Then transfer that remaining volume to a Mason jar and freeze for a good long time. Try not to peek. When it comes time to pour the solvent off into the filter, move rapidly.I hope some of this helps. Please don't hesitate to keep us posted.
Yes, I use glass for freeze precipitation - pint sized Mason jars typically.
I think your first "failure" may not have been one. Maybe you didn't get a big yield and it all kind of disappeared in the filter. Did you try evaporating all of the remaining solvent to see if you wound up with some DMT?
I have never done an ACRB extraction. And yet your problem is one I have heard described with MHRB. Maybe try turning your freezer up. That and/or leaving your jar in longer - and put it in the back right where the freezing air comes in.
Also, BEFORE placing DMT containing naphtha in your freezer, evaporate off about 1/2 the total volume. Then transfer that remaining volume to a Mason jar and freeze for a good long time. Try not to peek. When it comes time to pour the solvent off into the filter, move rapidly.
I hope some of this helps. Please don't hesitate to keep us posted.