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From my tests, it seems the higher alcohol solvents (99.9%IPA and 95% Everclear) are separating more or at least faster.
My updated best guesses at quantities from my 20g tests, incorporating extra steps from Transform:

20g MHRB in 100-150ML Ethanol or IPA (Alcohol 70 proof or higher)
Magnetic Stir/Hotplate for 6-12 hours (or more)
Allow to settle. Pipette off alcohol and set aside.
Mix another 100Ml Ethanol or IPA into your plant material
Magnetic Stir/Hotplate for another 6-12 hours (or more)
Allow to settle. Pipette off alcohol and strain/squeeze plant material through filter/fabric, to catch all the alcohol. Discard plant material.
Add 15-20g lime to the 200-250ml alcohol, mix again and let settle for at least 12 hours (settling in the freezer may be useful, though mine seemed to settle & separate more at room temperature)
You'll get a layer of DMT suspended in ethanol/alcohol up top and a layer of Calcium Tannate on the bottom
Pipette-off your ethanol/Alcohol. Discard Calcium Tannate
Evaporate as much as you want, depending on your chosen ROA

Transform: Any suggestions for how to ensure you're getting all the lime out of the finished product? Also, I'm going to add NaOH and naptha to the leftover Calcium Tannate layer to try to discern how much DMT is in there. It'd be nice to squeeze all the alcohol from that layer, but when I've tried, the lime/calcium ends up in my final product, passing through both coffee filters and makeup removal pads. I'd love help with this, as Colorado's state law has essentially limited legal DMT Extraction solvents to water, alcohol/ethanol, and limonene, so we're incentivized to perfect these teks that avoid Naptha and similar solvents.

<blockquote data-quote="Denverevolution" data-source="post: 3939473" data-attributes="member: 56423">From my tests, it seems the higher alcohol solvents (99.9%IPA and 95% Everclear) are separating more or at least faster. My updated best guesses at quantities from my 20g tests, incorporating extra steps from Transform:20g MHRB in 100-150ML Ethanol or IPA (Alcohol 70 proof or higher)Magnetic Stir/Hotplate for 6-12 hours (or more)Allow to settle. Pipette off alcohol and set aside.Mix another 100Ml Ethanol or IPA into your plant material Magnetic Stir/Hotplate for another 6-12 hours (or more)Allow to settle. Pipette off alcohol and strain/squeeze plant material through filter/fabric, to catch all the alcohol. Discard plant material.Add 15-20g lime to the 200-250ml alcohol, mix again and let settle for at least 12 hours (settling in the freezer may be useful, though mine seemed to settle &amp; separate more at room temperature)You&#039;ll get a layer of DMT suspended in ethanol/alcohol up top and a layer of Calcium Tannate on the bottomPipette-off your ethanol/Alcohol. Discard Calcium Tannate Evaporate as much as you want, depending on your chosen ROATransform: Any suggestions for how to ensure you&#039;re getting all the lime out of the finished product?&nbsp; Also, I&#039;m going to add NaOH and naptha to the leftover Calcium Tannate layer to try to discern how much DMT is in there. It&#039;d be nice to squeeze all the alcohol from that layer, but when I&#039;ve tried, the lime/calcium ends up in my final product, passing through both coffee filters and makeup removal pads. I&#039;d love help with this, as Colorado&#039;s state law has essentially limited legal DMT Extraction solvents to water, alcohol/ethanol, and limonene, so we&#039;re incentivized to perfect these teks that avoid Naptha and similar solvents.</blockquote>

[QUOTE="Denverevolution, post: 3939473, member: 56423"] From my tests, it seems the higher alcohol solvents (99.9%IPA and 95% Everclear) are separating more or at least faster. My updated best guesses at quantities from my 20g tests, incorporating extra steps from Transform: 20g MHRB in 100-150ML Ethanol or IPA (Alcohol 70 proof or higher) Magnetic Stir/Hotplate for 6-12 hours (or more) Allow to settle. Pipette off alcohol and set aside. Mix another 100Ml Ethanol or IPA into your plant material Magnetic Stir/Hotplate for another 6-12 hours (or more) Allow to settle. Pipette off alcohol and strain/squeeze plant material through filter/fabric, to catch all the alcohol. Discard plant material. Add 15-20g lime to the 200-250ml alcohol, mix again and let settle for at least 12 hours (settling in the freezer may be useful, though mine seemed to settle & separate more at room temperature) You'll get a layer of DMT suspended in ethanol/alcohol up top and a layer of Calcium Tannate on the bottom Pipette-off your ethanol/Alcohol. Discard Calcium Tannate Evaporate as much as you want, depending on your chosen ROA Transform: Any suggestions for how to ensure you're getting all the lime out of the finished product? Also, I'm going to add NaOH and naptha to the leftover Calcium Tannate layer to try to discern how much DMT is in there. It'd be nice to squeeze all the alcohol from that layer, but when I've tried, the lime/calcium ends up in my final product, passing through both coffee filters and makeup removal pads. I'd love help with this, as Colorado's state law has essentially limited legal DMT Extraction solvents to water, alcohol/ethanol, and limonene, so we're incentivized to perfect these teks that avoid Naptha and similar solvents. [/QUOTE]