Samvidbuho
Rising Star
Hello esteemed community:
I’ve been wanting to try out some ion exchange resins for upcoming product isolation, but haven’t pushed myself to actually experiment with this yet. At the moment I’m planning a DOE, but since this would be my first go I was hoping somebody more knowledgeable than me could check it and provide some constructive feedback if applicable.
Initial thoughts: (Starting materials: MHRB)
Begin with standard A/B. After the acidification stage is complete,
Immerse: 1 teabag full of Amberlite IRC-50 ion exchange resin (WCX) and 1 teabag full of Amberlite IRA-67 ion exchange resin (WAX). Soak overnight.
Elute the teabag containing the IRC-50 with basified water, then extract with organic.
I think it really is this simple, but also…
is it really this simple??
Appreciation in advance !
I’ve been wanting to try out some ion exchange resins for upcoming product isolation, but haven’t pushed myself to actually experiment with this yet. At the moment I’m planning a DOE, but since this would be my first go I was hoping somebody more knowledgeable than me could check it and provide some constructive feedback if applicable.
Initial thoughts: (Starting materials: MHRB)
Begin with standard A/B. After the acidification stage is complete,
Immerse: 1 teabag full of Amberlite IRC-50 ion exchange resin (WCX) and 1 teabag full of Amberlite IRA-67 ion exchange resin (WAX). Soak overnight.
Elute the teabag containing the IRC-50 with basified water, then extract with organic.
I think it really is this simple, but also…
is it really this simple??
Appreciation in advance !