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Wow! SWIM was thinking on this method lately, SWIM dissolved 25g sodium carbonate in 100ml waterthen added 100ml acetone. The acetone separated forming a cloudy layer on top, containing acetone, water and sodiun carbonate. This was left to sit overnight and the next morning the acetone layer was clear, having absorbed some water and sodium carbonate. The pH of this mixture was reaching 12.5-13 (the reading was really jumpy!).SWIM was thinking to extract MHRB this way and get all the alkaloids freebased and in the embrace of acetone. SWIM's currently thinking how he could proceed after that, possibly salting the alkaloids out of this mixture using fumaric acid.
Wow! SWIM was thinking on this method lately, SWIM dissolved 25g sodium carbonate in 100ml waterthen added 100ml acetone. The acetone separated forming a cloudy layer on top, containing acetone, water and sodiun carbonate. This was left to sit overnight and the next morning the acetone layer was clear, having absorbed some water and sodium carbonate. The pH of this mixture was reaching 12.5-13 (the reading was really jumpy!).
SWIM was thinking to extract MHRB this way and get all the alkaloids freebased and in the embrace of acetone. SWIM's currently thinking how he could proceed after that, possibly salting the alkaloids out of this mixture using fumaric acid.
