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Swim was planning on a cross between A/B and a STB...acidify rootbark to pH2 in crockpot for a given time to pull alkaloids into sltndump entire sltn including powdered rb into vesselbasify to pH 14+add appropriate amount of DCMlightly agitatedrain off DCM from the bottom of vesselcouple of quick, very mildly basic washes with H2OevapSwim is looking for full spectrum of alkaloids and will only recrystalize final product with warm heptane if he cant get the vapped DCM to solidify.Unless the powdered rootbark suspended in the aqueous sltn falls down into the DCM layer, swim doesnt see where filtering would be nessisary during any point of this extraction.If it does.... that would suck big hairy ones.
Swim was planning on a cross between A/B and a STB...
acidify rootbark to pH2 in crockpot for a given time to pull alkaloids into sltn
dump entire sltn including powdered rb into vessel
basify to pH 14+
add appropriate amount of DCM
lightly agitate
drain off DCM from the bottom of vessel
couple of quick, very mildly basic washes with H2O
evap
Swim is looking for full spectrum of alkaloids and will only recrystalize final product with warm heptane if he cant get the vapped DCM to solidify.
Unless the powdered rootbark suspended in the aqueous sltn falls down into the DCM layer, swim doesnt see where filtering would be nessisary during any point of this extraction.
If it does.... that would suck big hairy ones.