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Is this from the vendor from Mexico?A defat really should have taken care of almost all of the oils. Sounds like what you got was very oily.Do a recrystalization but if you can, try a sodium bicarbonate wash while your spice is in a NP solvent, I have noticed that the baking soda wash will take out some of the oils as well. It may take a few recrystalizations, but you can get oily goop into white/clear crystals.Anyone else have any ideas?
Is this from the vendor from Mexico?
A defat really should have taken care of almost all of the oils. Sounds like what you got was very oily.
Do a recrystalization but if you can, try a sodium bicarbonate wash while your spice is in a NP solvent, I have noticed that the baking soda wash will take out some of the oils as well. It may take a few recrystalizations, but you can get oily goop into white/clear crystals.
Anyone else have any ideas?