Tangarine_Dreams
Rising Star
TL/DR: 15min tek for clear to white spice.
fresh from the lab!
Materials:
100g pre powdered MHRB
100g Lye crystal
600ml distilled water
75ml of bestine brand or similar pure heptane.
long pipette of syringe with tube attached.
750ml alcohol bottle or similar glass seal-able vessel.
1. over the course of 10min add lye to water in the bottle. shake and stir very well. be sure to vent from time to time. i run it under a gently cool water sink just in case. but you CANNOT let it get cold. once all 100g have dissolved and the water has cleared from it's cloudy state move to step 2.
2. using a funnel add 100g of mhrb. shake bottle to mix. when shaking in this step and the prior remember that hot liquid in a closed bottle causes the air inside to expand. avoid spraying your hands with basic liquid when unscrewing cap. the bottle should be warm to hot at this point. just avoid simmering the water.
3. immediately add the 75ml of heptane and shake like mad. heptane does not dissolve dmt well when anything but boiling. if you have done steps 1 and 2 correct the heat from the basic root mixture is enough to do this.
4. let the bottle settle for 5 or so min. i place my bottles on the subwoofer of my computer. 2min of dubstep is enough to break any emulsion ive seen yet. it also makes the solvent separate much much faster. heptane also seems to split faster than naphtha with a normal stb.
5. at this point the heptane should be on top and not have any black gew floating in it. it may appear cloudy or bubbly or something of the sort. this is(should be) the heptane boiling. but you deff dont want any bubbles of dark liquid. using your suction device remove most of the heptane. i can get about 65-70ml of the initial 75ml before it is too annoying to continue. never risk the purity of your 70ml of pure solvent for that last 5ml. we shall see it again anyway ;]
5.5 the second you suck the heptane into your pipette it should become VERY cloudy. almost totally opaque. this is the deadman's test to see if you ran this tek correct. the heptane should been hot enough in the bottle to dissolve huge amount of dmt, but as soon as it hits the pipette it will cool enough that the dmt will begin to fall out of solution causing the color shift.
6. place the solvent in a lidded non reactive jar and place in the freezer. in my experience due to the saturation of suddenly non soluble dmt, just 3min in the frz and you can see crystals growing(not just precipitating but growing like real crystals should). after one night in the coooooold freezer(cold enough that my veggies freeze in the fridge!)
7.pour the heptane into a beaker taking care to pour slow enough to not wash all free floating crystals out. most all your dmt should be stuck to the jar pretty good. not like a naphtha FP, but actually caked on and stuck to the jar. you can now pour this cleanish heptane back into your bottle of basic liquid.
I am able to do this start to finish in 15min plus the night in the freezer. it yields pure clear to white to slightly off white crystals. most of which stay separate in the jar so if you take care scraping you can keep them apart.
this tek depends on a few key things.
-saving the heat energy from the basification to boil your naptha.
-pre powdered mhrb does not need more than 5min in solution to break down the cellulose and free the dmt.
-using heptane.
-woofer helps seperate while remaining HOT!
for your second pull i suggest capping your bottle with the base liquid and heptane and running it under a sink for 20min. most household sinks will hit 180 or atleast 140 which is enough to boil the heptane. i do not know the effects of letting the heptane soak in the bottle for more than a couple min. contam may go up.
after 2 or 3 pulls i switch to naphtha and do your normal normans tek to pull spice. a combo of cooling pulls durring FP will ensure no oils. to do this siphon off the solvent after 10-20min in the frzr. place the yellow solvent in a clean jar and continue the FP. once the orange/brown goop has fallen out but not the dmt. this yields a crystalline/fluffy yellow spice. if you dry the goop you get orange spice.
i save my goop in a jar and am growing red crystals in brown oils atm.
fresh from the lab!
Materials:
100g pre powdered MHRB
100g Lye crystal
600ml distilled water
75ml of bestine brand or similar pure heptane.
long pipette of syringe with tube attached.
750ml alcohol bottle or similar glass seal-able vessel.
1. over the course of 10min add lye to water in the bottle. shake and stir very well. be sure to vent from time to time. i run it under a gently cool water sink just in case. but you CANNOT let it get cold. once all 100g have dissolved and the water has cleared from it's cloudy state move to step 2.
2. using a funnel add 100g of mhrb. shake bottle to mix. when shaking in this step and the prior remember that hot liquid in a closed bottle causes the air inside to expand. avoid spraying your hands with basic liquid when unscrewing cap. the bottle should be warm to hot at this point. just avoid simmering the water.
3. immediately add the 75ml of heptane and shake like mad. heptane does not dissolve dmt well when anything but boiling. if you have done steps 1 and 2 correct the heat from the basic root mixture is enough to do this.
4. let the bottle settle for 5 or so min. i place my bottles on the subwoofer of my computer. 2min of dubstep is enough to break any emulsion ive seen yet. it also makes the solvent separate much much faster. heptane also seems to split faster than naphtha with a normal stb.
5. at this point the heptane should be on top and not have any black gew floating in it. it may appear cloudy or bubbly or something of the sort. this is(should be) the heptane boiling. but you deff dont want any bubbles of dark liquid. using your suction device remove most of the heptane. i can get about 65-70ml of the initial 75ml before it is too annoying to continue. never risk the purity of your 70ml of pure solvent for that last 5ml. we shall see it again anyway ;]
5.5 the second you suck the heptane into your pipette it should become VERY cloudy. almost totally opaque. this is the deadman's test to see if you ran this tek correct. the heptane should been hot enough in the bottle to dissolve huge amount of dmt, but as soon as it hits the pipette it will cool enough that the dmt will begin to fall out of solution causing the color shift.
6. place the solvent in a lidded non reactive jar and place in the freezer. in my experience due to the saturation of suddenly non soluble dmt, just 3min in the frz and you can see crystals growing(not just precipitating but growing like real crystals should). after one night in the coooooold freezer(cold enough that my veggies freeze in the fridge!)
7.pour the heptane into a beaker taking care to pour slow enough to not wash all free floating crystals out. most all your dmt should be stuck to the jar pretty good. not like a naphtha FP, but actually caked on and stuck to the jar. you can now pour this cleanish heptane back into your bottle of basic liquid.
I am able to do this start to finish in 15min plus the night in the freezer. it yields pure clear to white to slightly off white crystals. most of which stay separate in the jar so if you take care scraping you can keep them apart.
this tek depends on a few key things.
-saving the heat energy from the basification to boil your naptha.
-pre powdered mhrb does not need more than 5min in solution to break down the cellulose and free the dmt.
-using heptane.
-woofer helps seperate while remaining HOT!
for your second pull i suggest capping your bottle with the base liquid and heptane and running it under a sink for 20min. most household sinks will hit 180 or atleast 140 which is enough to boil the heptane. i do not know the effects of letting the heptane soak in the bottle for more than a couple min. contam may go up.
after 2 or 3 pulls i switch to naphtha and do your normal normans tek to pull spice. a combo of cooling pulls durring FP will ensure no oils. to do this siphon off the solvent after 10-20min in the frzr. place the yellow solvent in a clean jar and continue the FP. once the orange/brown goop has fallen out but not the dmt. this yields a crystalline/fluffy yellow spice. if you dry the goop you get orange spice.
i save my goop in a jar and am growing red crystals in brown oils atm.
