■PanoraMIX European AB and Xylene

[dmt005]

Ok so an extraction was performed by SWIM using the ■PanoraMIX European AB. This tek was followed exactly. Extraction was scaled up to 200g instead of 100 thus all following steps were increased accordingly.

SWIM was able to retrieve maybe 1g out of this maybe a little more. This tek is supposed to yield around 2g per 100g rootbark from what I have been told. Rootbark was from http://www.adenium.com.br/mimosa.asp

After Naptha pulls and only retrieving about 1g of spice swim decided to use a dif NP solvent to try and retrieve more. Xylene was chosen for this procedure. About 4 pulls of 50ml of Xylene were done and left to evap off to retrieve Crystal spice.

SWIM just checked and the only thing that is in her Pyrex dish is a clear oily substance that does not smell of spice and at the very bottom (Pyrex dish was placed at an angle) there is a pool of oilyish stuff with a yellow tint and swirls of white. SWIM is thinking of doing a recrystallization using Naptha but wanted to get some input from her fellow hyperspace comrades before proceeding

 

[dmt005]

?????????????????????

 

[Hupecat]

i am stuck at the same position actually...

Last time it tried to pull with Xylene, i only got this globby yellow blob.....
which istarted to rex with naphta, but after completely slow evap, theres nearly nothing left over in the dish... and i had 4 gr of goo in it....
so, not sure to go on with Xylene once again, or wait for my Heptan..

So, my Bestine has arrived...
i i will end pullimg Xylene today,...
Bit scared, cause after following a rex-tek before, i completely let 1,5 gr of light yellow spice disappeari had one glass which i evaporated, just a bit of goo at he ground.. rest ist gone..
the other glas didnt precipate correctly in freezer with Naphta... so, will tryout a rex with some bestne today...is there anybody out there who mihjt know an idiots guide for an easy rex.. i know it sounds easy as 1, 2, 3, but i always got left over woth nothing!!!!
I need a 100% idiotsafe pictorial wouldbe best.....

i triedthis one with naphta, and had no results, except those tiny little yellow blobs at the bottom

my initial naphta pulls came out fine... maybe they should be rexed as well, but atm i have a dish full of milkly xylene..
i know i would need some Fumaric Acid some day.., but not easy to obtain in germany... and i dont wanna order a 2,5 kilo bag from the US,, what for=?
Can i just "salt out" the pulled Xylol by adding a few drops of vinegar and a few drops of water and then freeze?
dont wanna kick all my shit into the bin this time....