I am using stb extraction method and making dmt. Once crystallization is finished, I do the mini-ab washing method and then sodium carbonate washing.
I am having trouble with dmt crystals precipitating between the non-polar solvent and the sodium carbonate during the sodium carbonate wash. Recently, the precipitation of dmt crystals has become worse over time, so we are attempting to extract as quickly as possible. Is there any way to prevent this precipitation? Recently, I thought that using a aliquot funnel instead of a dropper might improve the situation, so I purchased a aliquot funnel.
I am having trouble with dmt crystals precipitating between the non-polar solvent and the sodium carbonate during the sodium carbonate wash. Recently, the precipitation of dmt crystals has become worse over time, so we are attempting to extract as quickly as possible. Is there any way to prevent this precipitation? Recently, I thought that using a aliquot funnel instead of a dropper might improve the situation, so I purchased a aliquot funnel.
