the first pull i put into a small dish and into the  freezer for 20 minutes. then i decanted it and added the next pulls to it.

i put the total of the puls into my large dish and into the freezer for some 5-6h, i dont know precisely.

at this point, the spice in the small dish was gone, it was not much. so i decanted the container in the freezer into the now mostly empty small dish to put it back into the freezer.

when i blew onto the naphta at this point, it became milky.