• Members of the previous forum can retrieve their temporary password here, (login and check your PM).

Thanks Dg

Migrated topic.

antichode

Esteemed member
Joined
May 8, 2009
Messages
479
Merits
48
Not sure if I ever said it before now, but thanks for your contribution to these forums over the years. If it wasn't for you my mescaline definitely wouldn't look this purdy!

This is from 350 grams of powdered Pachanoi
STB with KOH
Pulled with xylene, heat and a lot of patience.
Sulfate salts
Yield = 5.9 grams
 

Attachments

  • 01.png
    01.png
    390 KB · Views: 0
Sweet pic antichode! Well done :want:

Yes this is a HUUUUUGE THANK UU!! to dg.
My thanks to dg and his knowledge is long overdue & apperciated
 
Very nice - and a good yield for the sulfate tek!

If I may ask, was this pachanoi you grew? Almost 2% seems high for commercially available pachanoi, unless you got it from South America.

Also, if you wouldn't mind, could you describe your titration / pulling process in some detail? I'm thinking my friend may not be getting everything out of his solvent.
 
xram said:
Very nice - and a good yield for the sulfate tek!

If I may ask, was this pachanoi you grew? Almost 2% seems high for commercially available pachanoi, unless you got it from South America.

Also, if you wouldn't mind, could you describe your titration / pulling process in some detail? I'm thinking my friend may not be getting everything out of his solvent.

Hey xram... This was Pachanoi that I grew. I have about 20 mature plants and over the years Ive weeded out the low performers. This was dry flesh but no spine, everything else though, skins and all.

The titration is just the one that Dg has promoted on here. just add dilute sulphuric acid till ph 7 is reached. You need to vigorously stir the saltings in between each addition. I use a good quality PH meter for this.

solvent extraction is somewhat tedious but just requires lots of heat. I use KOH mixed with water and blend it with the powdered cactus using a drill, then let it slake for a few days before adding solvent. Blend the solvent with a drill again (I use a coat hanger bent to form a mixer) and leave it in a hot water bath at 80 C until it separates. I do four solvent pulls and then salt once.

Interestingly my solvent pulls come off crystal clear when hot but when they cool they go cloudy, Im not sure what this precipitate is but it doesn't settle, even after one month in the fridge! The mescaline certainly doesn't seem to show any signs of base contamination and its plenty potent
 
Back
Top Bottom