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Looking back through this thread, two questions still deserve definite answers:- what is the yellow-fluorescing stuff in Endlessness' caapi tlc at the same rf as THH? Oleamide seems like a good candidate but a definitive analysis seems desirable. 2-d tlc would be a good place to start - rotate the plates by 90° and run them again with a different solvent system. The yellow stuff and the THH should resolve separately given the right solvents.- we still don't know if the two enantiomers of THH have different pharmacology - or if THH gets racemised under physiological conditions. Also, would a cold-extracted caapi THH sample be different from brewed caapi THH extracted after prolonged simmering? Is Callaway's claim based on experimental evidence?
Looking back through this thread, two questions still deserve definite answers:
- what is the yellow-fluorescing stuff in Endlessness' caapi tlc at the same rf as THH? Oleamide seems like a good candidate but a definitive analysis seems desirable. 2-d tlc would be a good place to start - rotate the plates by 90° and run them again with a different solvent system. The yellow stuff and the THH should resolve separately given the right solvents.
- we still don't know if the two enantiomers of THH have different pharmacology - or if THH gets racemised under physiological conditions. Also, would a cold-extracted caapi THH sample be different from brewed caapi THH extracted after prolonged simmering? Is Callaway's claim based on experimental evidence?
