An A/B extraction was done using acetic acid.

The orange came out on the third pull.

The solvent used was heptane which was heated to a nice self-bubbling near-boil before being added into an extremely hot water-bathed extraction vessel.

After mixing + separation the heptane layer was removed and put onto a pyrex baking dish and set in front of a small high-powdered fan to reduce.

Due to some DMT smoking going on at the time it was left too long, over-reduced and precipitate began to form + stick all over the bottom of the big pyrex baking dish. At this point, not particularly orange.

The pyrex was VERY cold after the reduction, condensation forming on the outside of it.

The little bit of heptane left was VERY cloudy and was freeze-precipitated to yield about .5g of the whitest most shiny crystalline white powder that the kitty has ever seen out of an initial freeze precipitation.

The pyrex baking dish was left in front of the fan overnight to completely dry and in the morning 2.2g of DMTang was there for the scraping.

:d