DonPeyote
Rising Star
This was my first time using Xylene as the NP solvent in an A/B extraction of Acacia Confusa.
500ml of Xylene was used per pull. Each pull was treated with dry ice to seperate the NMT from the DMT (The fourth pull was non-reactant, so all the DMT/NMT was extracted with 3 pulls).
927mg of fumaric acid was dissolved in 150mls. of anhydrous acetone, and mixed with the xylene/DMT. After 24 hours, crystals were noticeable. The solution was poured through a filter to collect the DMT fumarate, which was washed 4 times with acetone. The result was a slightly salmon white 3.7grams DMT fumarate
The Xylene pulls were treated again, with 618mg fmaric acid/100ml acetone, to see if anything was left. Overnight a white precipitate formed, which was collected and washed in acetone 4 times. The result was 1.2 grams white DMT fumarate.
Pictures below.
Not sure I love xylene. It takes a lot of washing to get the smell out. However, it IS efficient at extracting DMT from ACRB, and delivering DMT fumarate ready to roll.
500ml of Xylene was used per pull. Each pull was treated with dry ice to seperate the NMT from the DMT (The fourth pull was non-reactant, so all the DMT/NMT was extracted with 3 pulls).
927mg of fumaric acid was dissolved in 150mls. of anhydrous acetone, and mixed with the xylene/DMT. After 24 hours, crystals were noticeable. The solution was poured through a filter to collect the DMT fumarate, which was washed 4 times with acetone. The result was a slightly salmon white 3.7grams DMT fumarate
The Xylene pulls were treated again, with 618mg fmaric acid/100ml acetone, to see if anything was left. Overnight a white precipitate formed, which was collected and washed in acetone 4 times. The result was 1.2 grams white DMT fumarate.
Pictures below.
Not sure I love xylene. It takes a lot of washing to get the smell out. However, it IS efficient at extracting DMT from ACRB, and delivering DMT fumarate ready to roll.
