Success! Good stuff. Excess shellite is definitely an issue when trying to precipitate. I for one make enhanced leaf so I don't even bother precipitating I simply evaporate straight after extraction. This yields allot higher as included in the goo is the oils, which are active, and I don't think absolutely all the DMT precipitates when you put it in the freezer anyway no matter how diluted it is, though I could be wrong. So really it's up to you, you could leave it in for an extra day then pour off the shellite and evaporate half and scrape up what was in the bowl, or melt the crystals back into the shellite then evaporate half, or just evaporate all of it. Let us know what happens..