Infundibulum said:Cosmic Lion, it would be uber-cool if SWIY dose the above analysis!
Even though I'm not quite sure how you'll use the mass spec to determine the pKa of THH. Why doesn't SWIY go for standard titration?
Titration would be ideal, actually.
SWIM is in the works of ordering some THH to run some solubility tests on. Going to dissolve it into a slightly acidic solution then titrate Sodium Carbonate dropwise until precipitation occurs. SWIM might be able to get a chemical color indicator to put in solution to help signal when the proper pH is reached.