Bufo 1:4 cleanup gone wrong?

[clearlyone]

Used the Bufotenine IPA Extraction and Bufojam Changa Tek with hopes to then clean with acetone/naptha at 1:4 ratio.

Tek itself went smoothly yielding 540mg of dark caramel, slightly sticky product from 8g cebil seeds.

220mg of the product was then to be dissolved in 15ml acetone. Much dissolved, but a substantial amount would not dissolve with considerable mixing. More acetone was added for a total of about 30ml. Still most remains would not dissolve. Naptha was then added to achieve 1:3 acetone/naptha. This was mixed a minute or so then decanted. This is now evaporating.

Is it OK that some dark product would not dissolve in the Acetone? (it was saved)

Not sure what to expect from the acetone/naptha evaporation?

Are there simple wash options for cleaning the nasties out of the freebase obtained with the Tek?

 

[clearlyone]

Hmmm...

Of the original 220mg from the tek, 110mg did not dissolve in the acetone. So it would seem the acetone/naptha picked up about 110mg. This evaporated leaving 38mg of dark caramel freebase. Not sure there has been any purification.

Debating next steps. Could one dissolve in acetone (as best it can be made to) then salt with FASA? Seems there may already be too many plant fats to dissolve ... but would they keep the bufo trapped?