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Update.SWIM's never seen a yield that high (not even from 250g of MHRB).Given that a lot of it is particles that went through the T-shirt filter....and that it might be a little dirtier due to trace amounts of water....but after 4-5 washes or acetone, and then a MEK:Heptane wash....should be very pretty.Update on the orange supernatant. After letting it sit for ~7 hours, swim noticed that it is in fact white precipitate giving it the orange translucency. He noticed that about about 1/8th of it settled, and saw very clear yellow-orange acetone. SWIM just poured off this supernatant, and will let it sit as it is, the white powder will eventually settle. SWIM will also try adding more FASA to it, since it most likely has more alkaloids in it. Either way, the massive amount of filthy crystals in the test tubes is very satisfying.E.C.EDIT: Now consolidated into 1 test tube. This stuff settles so quickly. SWIM has a feeling though that even after his acetone is near clear, the crystals will still be brown and disgusting. SWIM's praying for MEK:Heptane to do the trick.Consolidated:Can't really tell from the picture, but the acetone is a piss-yellow color.
Update.
SWIM's never seen a yield that high (not even from 250g of MHRB).
Given that a lot of it is particles that went through the T-shirt filter....and that it might be a little dirtier due to trace amounts of water....but after 4-5 washes or acetone, and then a MEK:Heptane wash....should be very pretty.
Update on the orange supernatant. After letting it sit for ~7 hours, swim noticed that it is in fact white precipitate giving it the orange translucency. He noticed that about about 1/8th of it settled, and saw very clear yellow-orange acetone. SWIM just poured off this supernatant, and will let it sit as it is, the white powder will eventually settle. SWIM will also try adding more FASA to it, since it most likely has more alkaloids in it. Either way, the massive amount of filthy crystals in the test tubes is very satisfying.
E.C.
EDIT: Now consolidated into 1 test tube. This stuff settles so quickly. SWIM has a feeling though that even after his acetone is near clear, the crystals will still be brown and disgusting. SWIM's praying for MEK:Heptane to do the trick.
Consolidated:
Can't really tell from the picture, but the acetone is a piss-yellow color.