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I think DMT is too soluble to effectively FP in DCM. Maybe if you reduced it to the saturation point you'd be able to get some crystals that way...If I were SWIM, I would distill most of the volume, then evap the rest and redissolve in Naptha for a freeze precip. Don't try and evap it completely thru distillation - I think it might oxidize it or something. It's alright to have a little DCM mixed in with the naptha when you FP.
I think DMT is too soluble to effectively FP in DCM. Maybe if you reduced it to the saturation point you'd be able to get some crystals that way...
If I were SWIM, I would distill most of the volume, then evap the rest and redissolve in Naptha for a freeze precip. Don't try and evap it completely thru distillation - I think it might oxidize it or something. It's alright to have a little DCM mixed in with the naptha when you FP.
