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huge crystal masses appearing in only two hours in refrigerator!

1Starway7

Established member
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trying slow evaporation method ...

interesting online find.... photos of 500 gram extraction of acacia bark from the big island.. this is barely 1/3rd of the bark ... and want to show what happened to some napatha pulls that were just sitting in a cabnet at room temperature...what happened when they put it in a small dorm refrigerator with only the top of jar touching the bottom of the tiny freezer!
jpg 502;'' agressive white crystals... forming in just two hours!!:giggle:...is this posible without being in a freezer?


jpg...503 and 504...after 5 hours...

they must be pulling a lot of the molecule..... their plan... is to turn all 500 grams into a much cleaner [D]... molecule citrate for long storage ...by letting it migrate into a citrate water then evaping all the water out...

Had there been less napatha in the mix . the results would have been better.....because in morning..... a lot of crystals were still stuck to glass... but there was a lot of new floating crystals...

this doesnt really matter ....because once... citrate water...is mixed into the uncleaned napatha pulls...cleaning it further ...then seperate out the acidic water .... then totally evaporate the water out...

... and after drying for a few days being left with much dryer ...D.citrate beads.... that should store for years if kept in dark cool areas like a cabnet or closet..
even if the citrate beads melt inside a capsule they are still active...The molecule is ancient ..it takes a lot to destroy it!

this method by letting top of jar touch the the coldest lowest spot in freezer ..it kinda made the glass jar..... [ that was way too big to fit into small freezer]....into a freezer jar/...and it worked!

the D. beads are fine for oral use and posibly?....vaporizable?. depending on how much citric acid was used....?


... then later...... if one wants freebase.....turning the citrate beads back into freebase..[even into a single vapable dose]..... is a simple mater of mixing some beads into distilled water...then a small measured amount of lye added into a narrow test tube capped bottle......then a layer of fresh napatha...shake the bottle ...then ....
[after seperation].......pipette out the fresh napatha layer...back into freezer ........

.[or fan dry ].... ..then viola!.... clean white D. freebase crystals to vaporize!

the last two photos taken from .....[trying slow evaporation method] ...[thread]....of dryed and hardened D ..citrate beads.....
 

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