SWIKiljosh
Rising Star
Hi I met this guy on an airplane. He talked my ear off for hours I fell asleep but I woke up and a note was on his seat, it read...
Combined 40g MHRB Powdered into quart jar. Seperately mixed 1g:15ml lye/water and stirred till all was dissolved. Added unknown amount of naptha, about a pinky width in a quart jar. Rolled and shook for about an hour. Placed in a crockpot of water, on a towel in the bottom. Heated on high for 2 hours, rolling every 15 minutes or so. Ratio was 1gBark:1gLye:15mLWater
Naptha pulled with an eye dropper into a hot tiny jar. This is where things went off course..
Placed dmt laden naptha into pyrex dish on a hot plate to evaporate down. Half hour later it was checked to find naptha had evaporated, only brown goo that was very liquidy(Naptha present still but barely.) Goo was smelled right but tasted of solvent and flamed up.
Goo was redissolved in a minimal amount of naptha and set to the side in Jar A. Second pull was done after roughly an hour sitting in a warm jar of NaOH/water. It was added to Jar B and placed on the hotplate to evap halfway. Once down halfway Jar A was added to B and evaped another 1/3. Color was a dark yellow that did not cloud when you blew on it. There was a small amount of brown goo that was on the bottom not fully settled but kind of floating while tethered down.
Placed in freezer after 5 or 10 minutes at room temp and it was surrounded with ice packs for good measure. Hope it was evaped enough.
A third pull was done after an additional 150ml of 1g:15ml lye/water was mixed in. The third pull is evaping at room temp in front of a fan set on exhaust out the window. Suspecting the heat used to evap caused the brown goo. The quart jar was set to the side to cool off with another pinky's worth of naptha to pull tomorrow.
Was he correct in his assumptions that evaporating naptha will produce a brown goo so a freeze precipitation should be done for crystal? How solid does this whole technique look? And is it necessary to defat if freeze precipitating?
In theory if you combined two pulls of 40gbark and you wanted to freeze precip how much naptha would be put in freezer? Around half a 4oz jelly jar? If I had the qualifications to do this Id be worried my solution wouldn't be saturated enough especially if no clouding happened when I blew on it.
Would you have to heat the solution back up for the 4th and final pull? Or will room temp Naptha pull ok.
If an Acetone defat was done prior to immersing in Lye water would evaping yield powder or is the goo caused by the heat or someting in the Naptha?
Thanks for any help I am very curious.
Combined 40g MHRB Powdered into quart jar. Seperately mixed 1g:15ml lye/water and stirred till all was dissolved. Added unknown amount of naptha, about a pinky width in a quart jar. Rolled and shook for about an hour. Placed in a crockpot of water, on a towel in the bottom. Heated on high for 2 hours, rolling every 15 minutes or so. Ratio was 1gBark:1gLye:15mLWater
Naptha pulled with an eye dropper into a hot tiny jar. This is where things went off course..
Placed dmt laden naptha into pyrex dish on a hot plate to evaporate down. Half hour later it was checked to find naptha had evaporated, only brown goo that was very liquidy(Naptha present still but barely.) Goo was smelled right but tasted of solvent and flamed up.
Goo was redissolved in a minimal amount of naptha and set to the side in Jar A. Second pull was done after roughly an hour sitting in a warm jar of NaOH/water. It was added to Jar B and placed on the hotplate to evap halfway. Once down halfway Jar A was added to B and evaped another 1/3. Color was a dark yellow that did not cloud when you blew on it. There was a small amount of brown goo that was on the bottom not fully settled but kind of floating while tethered down.
Placed in freezer after 5 or 10 minutes at room temp and it was surrounded with ice packs for good measure. Hope it was evaped enough.
A third pull was done after an additional 150ml of 1g:15ml lye/water was mixed in. The third pull is evaping at room temp in front of a fan set on exhaust out the window. Suspecting the heat used to evap caused the brown goo. The quart jar was set to the side to cool off with another pinky's worth of naptha to pull tomorrow.
Was he correct in his assumptions that evaporating naptha will produce a brown goo so a freeze precipitation should be done for crystal? How solid does this whole technique look? And is it necessary to defat if freeze precipitating?
In theory if you combined two pulls of 40gbark and you wanted to freeze precip how much naptha would be put in freezer? Around half a 4oz jelly jar? If I had the qualifications to do this Id be worried my solution wouldn't be saturated enough especially if no clouding happened when I blew on it.
Would you have to heat the solution back up for the 4th and final pull? Or will room temp Naptha pull ok.
If an Acetone defat was done prior to immersing in Lye water would evaping yield powder or is the goo caused by the heat or someting in the Naptha?
Thanks for any help I am very curious.