OriginalFace
Rising Star
No Smell, Quick and Easy, Almost Pure Bufotenine Extraction
Goal: Obtain pure bufotenine freebase from cebil seeds.
Materials:
* 20 grams cebil seeds
* coffee grinder
* mortar and pestle can be used for manual operation
* anhydrous acetone
* prepared by adding baked epson salts to store bought acetone
* naphtha
* water
* sodium carbonate, "pH up" for swimming pool is good.
* funnel for filtering.
* coffee filter.
* cotton ball.
* mason jars, 250 ml wide mouth are ideal.
* medicine dropper, 1 ml, as used with vitamin drops or kids medicine.
* turkey baster, graduated. Used to measure naphtha.
Procedure:
1. Weigh and grind whole cebil seeds to a fine powder using coffee grinder or mortar and pestle.
2. Add about 5 grams of sodium carbonate and mix to make a uniform mixture.
3. Add water slowly, bit by bit to make a doughy paste. Cover jar and let sit for an hour to allow reaction to complete. We are making a crude bufotenine freebase at this step, which contains bufotenine along with undesired, nausea producing compounds, as well as plant oils and fats
4. If the right consistency of paste was achieved in the previous step, then the sodium carbonate will have formed its hydrated state and we will be left with a hard dry cake. An ammonia smell will be apparent, indicating that the freebasing reaction has occurred. If an excess of water was used then just leave the jar uncovered and let the water evaporate away. Heat and a fan will speed up this operation. Bufotenine is very heat tolerant and the water could safely be boiled away if you are in a hurry.
5. Grind up the hard cake then cover with anhydrous acetone. The bufotenine will dissolve in the acetone forming a yellow solution while leaving behind any unused sodium carbonate behind. Pour off the acetone solution into a collection jar and repeat the process by adding more acetone for a total of three extractions.
6. Filter the combined three acetone extractions, through a cotton ball loosely stuffed in the narrow part of a funnel, to obtain a clear yellow acetone solution of crude bufotenine freebase.
7. Add the contents of a 500 mg fumaric acid capsule directly to this solution and observe an instantaneous crashing out of bufotenine fumarate. This is a defatting step and effectively removes the plant oils and fats. Let this sit for a while to allow the reaction to complete. The bufotenine fumarate will stick to the sides and bottom of the jar and the waste acetone containing the unwanted oils can be poured off. Allow any remaining acetone to evaporate away until its odour is gone.
8. Add enough water (about 50 ml) to dissolve the bufotenine fumarate then add about a gram of sodium carbonate powder directly to this solution. Like magic a caramel coloured lump of freebase bufotenine will form. This lump should be flattened out while adding an excess of water, to allow complete penetration by the sodium carbonate. Let this reaction continue for a while to completion, then pour off the water and dry out the caramel bufotenine.
9. Completely dissolve the impure bufotenine in 5 mL of acetone then add 20 ml of naphtha ( 1 part acetone : 4 parts naphtha ). This will crash out the unwanted nausea causing compounds leaving pure bufotenine in an almost clear solution. Allow the reaction sufficient time to complete.
10. Use the medicine dropper to siphon off the clear bufotenine solution to another jar, leaving behind the nausea nasties.
11. Evaporate the solvent to obtain light tan, reasonably pure bufotenine freebase.
Goal: Obtain pure bufotenine freebase from cebil seeds.
Materials:
* 20 grams cebil seeds
* coffee grinder
* mortar and pestle can be used for manual operation
* anhydrous acetone
* prepared by adding baked epson salts to store bought acetone
* naphtha
* water
* sodium carbonate, "pH up" for swimming pool is good.
* funnel for filtering.
* coffee filter.
* cotton ball.
* mason jars, 250 ml wide mouth are ideal.
* medicine dropper, 1 ml, as used with vitamin drops or kids medicine.
* turkey baster, graduated. Used to measure naphtha.
Procedure:
1. Weigh and grind whole cebil seeds to a fine powder using coffee grinder or mortar and pestle.
2. Add about 5 grams of sodium carbonate and mix to make a uniform mixture.
3. Add water slowly, bit by bit to make a doughy paste. Cover jar and let sit for an hour to allow reaction to complete. We are making a crude bufotenine freebase at this step, which contains bufotenine along with undesired, nausea producing compounds, as well as plant oils and fats
4. If the right consistency of paste was achieved in the previous step, then the sodium carbonate will have formed its hydrated state and we will be left with a hard dry cake. An ammonia smell will be apparent, indicating that the freebasing reaction has occurred. If an excess of water was used then just leave the jar uncovered and let the water evaporate away. Heat and a fan will speed up this operation. Bufotenine is very heat tolerant and the water could safely be boiled away if you are in a hurry.
5. Grind up the hard cake then cover with anhydrous acetone. The bufotenine will dissolve in the acetone forming a yellow solution while leaving behind any unused sodium carbonate behind. Pour off the acetone solution into a collection jar and repeat the process by adding more acetone for a total of three extractions.
6. Filter the combined three acetone extractions, through a cotton ball loosely stuffed in the narrow part of a funnel, to obtain a clear yellow acetone solution of crude bufotenine freebase.
7. Add the contents of a 500 mg fumaric acid capsule directly to this solution and observe an instantaneous crashing out of bufotenine fumarate. This is a defatting step and effectively removes the plant oils and fats. Let this sit for a while to allow the reaction to complete. The bufotenine fumarate will stick to the sides and bottom of the jar and the waste acetone containing the unwanted oils can be poured off. Allow any remaining acetone to evaporate away until its odour is gone.
8. Add enough water (about 50 ml) to dissolve the bufotenine fumarate then add about a gram of sodium carbonate powder directly to this solution. Like magic a caramel coloured lump of freebase bufotenine will form. This lump should be flattened out while adding an excess of water, to allow complete penetration by the sodium carbonate. Let this reaction continue for a while to completion, then pour off the water and dry out the caramel bufotenine.
9. Completely dissolve the impure bufotenine in 5 mL of acetone then add 20 ml of naphtha ( 1 part acetone : 4 parts naphtha ). This will crash out the unwanted nausea causing compounds leaving pure bufotenine in an almost clear solution. Allow the reaction sufficient time to complete.
10. Use the medicine dropper to siphon off the clear bufotenine solution to another jar, leaving behind the nausea nasties.
11. Evaporate the solvent to obtain light tan, reasonably pure bufotenine freebase.