ok so i went on to defat this ph 1.4 solution 3 times then basified to ph 13 and did 2 500ml naptha pulls in a hot water bath. during the freeze precip a lot a white crystal had formed but once i poured the solvent off most of the white stuff melted to a decent amount of yellow oil. what caused this? the low ph?

How should i clean this product up to get white spice?