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Please help! Might have pulled a little base into pyrex

Migrated topic.

Juliusx33

Rising Star
Merits
293
Ok so I’m doing a STB extraction and am on my third pull. When I used my pipette to suck the Heptane off, I think I got a drop or two of my bass (it was light brown). It looks clear now but how should I proceed from here? I have been putting my pulls in a glass dish thus far. Should I just continue and then re-crystalize?
 
DreadedShaman said:
It seems to me that you have the right idea, I would just finish my extraction and then re x to clean up anything

Thank you! I was going to instead after all my pulls, pour it all in a shot glass with base and separate again. However, there seems to be crystals already forming.
 
It looks like there is nothing there or a verry small amount of melted and not properly formed dmt solids that have melted?? so you should probably first try to yield a good enough amount of dmt if you are wanting to do a proper re x also if you have any naps in your dish you can always at the end before freeze pour your solvent from your dish you have base in into something else then wash the dish and dry and put it back or just use another dish 8)
 
BigJungleBuds said:
It looks like there is nothing there or a verry small amount of melted and not properly formed dmt solids that have melted?? so you should probably first try to yield a good enough amount of dmt if you are wanting to do a proper re x also if you have any naps in your dish you can always at the end before freeze pour your solvent from your dish you have base in into something else then wash the dish and dry and put it back or just use another dish 8)

Yeah that picture was after one pull because it was my first time using the pipette and I couldn't figure the damn thing out :oops: So crystals starting slowly forming because it starting evaporating quicker than I thought. Now have four pulls in the freezer and I checked recently, its looking gooooooood. After I freeze precipitate, going to Re x with some warm heptane :) Cheers :thumb_up:
 
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