I used the marsofold a/b tek on 1 KG Mimosa Powdered Pink Inner Root bark.
I went with a PH of 4(Distilled Water/White Vinegar) on the A step(1 Gallon-3to1 Ratio-Water/Vinegar per 500g)
and a PH of 13.4(Distilled Water+Lye -(1 Pint Water+70 G Lye)on the B step
Three Crock Pot simmers for 2 hours each stirred every 15 minutes
Decanted and vacum filtered all particles out before adding Lye
I extracted 3 times Using Lab grade Pet Ether for the Extractions(500 ML Each Extraction)
Reduced it to 20 % of original volume and Freeze precipitated
I kept each extraction seperate
First extraction resulted in off white xtals 7.5g
Second resulted in slightly yellow xtals 1.0g
third resulted in yellower X-tals .5g
I will do re-xtailization on each pull seperately...
I have found some help here on this outstanding forum in this post as follows...
Can anyone suggest some other links on recrystalization??
Thanks!!!!!
I went with a PH of 4(Distilled Water/White Vinegar) on the A step(1 Gallon-3to1 Ratio-Water/Vinegar per 500g)
and a PH of 13.4(Distilled Water+Lye -(1 Pint Water+70 G Lye)on the B step
Three Crock Pot simmers for 2 hours each stirred every 15 minutes
Decanted and vacum filtered all particles out before adding Lye
I extracted 3 times Using Lab grade Pet Ether for the Extractions(500 ML Each Extraction)
Reduced it to 20 % of original volume and Freeze precipitated
I kept each extraction seperate
First extraction resulted in off white xtals 7.5g
Second resulted in slightly yellow xtals 1.0g
third resulted in yellower X-tals .5g
I will do re-xtailization on each pull seperately...
I have found some help here on this outstanding forum in this post as follows...
Can anyone suggest some other links on recrystalization??
Thanks!!!!!
