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soxhlet exctracter

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That sucks,what happend? i think most of swims pieces arrived in the mail today ( i know the dig.hotplate did) but i'll find out tommorrow.Swim went a little nuts w/ the $ and purchased a bunch of helpful lab equp.You said that swiy uses a fish tank for the water? what size tank does he use ans what size water pump? swim is probably gonna do a mhrb extraction to sart and i read to use 91% API (Isopropyl Alcohol).What has swiy found to be effective?I was also was looking around the web for info on using a soxhlet on cannabus and others can you point me in a direction?
 
swim uses a large glass mixer bowl, and a small aquarium water pump. uses tygon tubing

IPA should work fine for MHRB, even EtOH (ethanol) would work well. swim would actually use ethanol (everclear).
ethanol is also good for extracting cannabinoids.

some people actually use butane to get 'honey oil' from cannabis. obviously couldn't get butane to cycle through a soxhlet, but hexane or heptane would.
 
swim bought a 500ml soxlhet w/condenser,flat bottom boil flask an a Cimarec® Digital Hot Plate 7.25 x 7.25 .Once swim gets it together it seems pretty basic and i likes the idea of using cotton balls as appose to a thimble.One question,though. Swim is used to a/b extractions (marsfold specifcally).That tek cals for 3/1 water vineger for the polar extraction (which the soxhlet does more efficiently for you).Why is it best to use IPA or EVERCLEAR as appose to what some of the other teks use,for instance; Vovins polar is distilled h20 and hydrochloric acid.why does api and eveclear seem to work better w/ soxlet the some of the other solvents?
 
Why not just use a stovetop? saves a bit of money.
Swims busy using the stove, but the flask is in a hot water bath. Hes a bit scared of it shattering from the heat, bust since its proper lab glass, it shouldn't right?

Swims sick of all the water vapours going everywhere all the time, think hes vapored away about 10L today.

Also what solvents do you guys use?
SWIMs trying it with naptha tonight, because hes so excited about getting his new soxhlet from the US. (not the big 1000ml yet though),

Swim actually bought 4 soxhlet bodies off e-bay just because they were so cheap. He'll have to sell them again, so if there are any aussies looking to get into it, message me.
 
i believe it was you benzyme that said if swim was doing 500g mhrb extractions that a 500ml soxhlet would be sufficient.Obviously the most organic material swim can extract would be how much he can fit into the soxhlet,or should there be xtra room left,How much generally (at max) root bark can you fit into 500ml.Also what about minimum amounts of material.With 500ml, would it make a difference if say you only wanted to do a 50-100g extraction,does that change anything?
 
The only thing that matters is that you have enough solvent to fill the Soxhlet completely or it will never siphon.
 
Can swim buy IPA or EVERCLEAR at most harware stores?he's never used it before. Also 69ron you mentioned that when swim is done w/ the polar extraction,using the soxhlet he can continue to follow whatever tek he chooses,is that correct?
 
Dwhitty76 said:
Can swim buy IPA or EVERCLEAR at most harware stores?he's never used it before. Also 69ron you mentioned that when swim is done w/ the polar extraction,using the soxhlet he can continue to follow whatever tek he chooses,is that correct?
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IPA can be obtained at a pharmacy. denatured alcohol can be obtained at a hardware store. everclear is found at liquor stores
 
benzyme said:
69ron said:
The only thing that matters is that you have enough solvent to fill the Soxhlet completely or it will never siphon.
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it just needs to fill to the level of the top of the inner siphon, which (depending on the extractor) may be well below the top of the outer siphon
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Exactly...and the amount varies according to how dense the plant material is. Actually I was a little incorrect in my statement. The general rule is like this:

Before starting the system, fill Soxhlet with cotton balls, add plant matter, cover with cotton balls. Add enough solvent to cause the Soxhlet to siphon once into the boiling flask. Then add solvent to fill the Soxhlet 1/2 way to the siphon point. For example, if it took 300 ml to cause a siphon, then add 150 ml more. That's the general rule anyway. It varies a little according to the solvent used. DCM, for example usually requires more solvent than IPA, or it won't siphon properly. If at any time it fails to siphon while the system is running, adding a little more solvent usually solves the problem.

There are cases when it won't siphon at all for many hours even after adding more solvent. This is usually because the drainage is inadequate (if the plant is too finely powdered and DE wasn’t added) and so it will just drip endlessly down from the Soxhlet’s siphon arm (the small tube) into the boiling flask. If this happens and the solvent level stays at the siphon arm, don’t worry, it is still extracting. It doesn’t actually need to siphon. As long as it is dripping back down, it is extracting.

But, if at any time the solvent level in the Soxhlet starts to reach the distillation arm (the larger tube) then you’re in trouble. This means the system is clogged. You should turn it off. Remove the plant material, replace any cotton with new cotton, and add DE to the material to prevent it from clogging again. Then put it back in the Soxhlet. This is almost never a problem if the plant material is coarsely ground, and often a problem if the plant material is very fine powder.

Remember if you are using very fine plant powder then add DE to it. This works really well to prevent clogging.
 
Can someone please tell me if its possible to use Naptha or Ethanol for extraction? Or are you better off finding Methanol?
 
D_Juggz said:
Can someone please tell me if its possible to use Naptha or Ethanol for extraction? Or are you better off finding Methanol?
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depends on the procedure you want to use.

if you want to do a relatively quick pre-extraction like this thread addresses, you'd use hot ethanol, methanol, or isopropanol.
if you wish to soak or simmer the material with acidic water, you'd basify that, then add naptha.
 
Swim tried the acidic water, but couldn't get it to boil in my hot water bath, Tried it with naptha also, and it did seem to turn yellow after about 4-6 hours, but there is a little bit of water at the bottom that must have came from the plants, its also turned dark, is it possible that there is DMT trapped in that water? Should it be siphoned off before continuing?

So you say 95% Ethanol (what Swim has available) would work better than naptha? Wouldn't it be worse because its polar instead of the nonpolar methanol?
 
D_Juggz said:
Swim tried the acidic water, but couldn't get it to boil in my hot water bath, Tried it with naptha also, and it did seem to turn yellow after about 4-6 hours, but there is a little bit of water at the bottom that must have came from the plants, its also turned dark, is it possible that there is DMT trapped in that water? Should it be siphoned off before continuing?

So you say 95% Ethanol (what Swim has available) would work better than naptha?
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you don't want it to boil, just use low heat. DMT is quite soluble in acidic water, heat increases the solubility. but boiling can break down the alkaloids. gentle heat for a few hours or even overnight is more than enough.
likewise with alcohols, though even shorter timeframe. DMT is quite soluble in short-chained aliphatic alcohols, which require even less heat. and yes..DMT, straight from the root bark, is more soluble in ethanol than naptha.

you don't use naptha (unless you want to defat..which is optional, not really necessary) until after you basify the acidic solution.
 
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