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Nothing has been ruined by adding too much nps, as far as I am aware. I'm not sure about it taking longer to separate, but I can't read the Reddit page, so I'm not sure whether the tec is stb or acid-base. If it's stb then maybe all the bark in the soup is causing this emulsion.

As far as I'm aware, the only issue here is that the NPS will have a much lower concentration of dmt, and so you won't have so much precipitating out when freezing.

Don't sweat it, and don't waste all the nps evaping. I never purposely evap any solvent, just keep it and use for the next pull.


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