• Members of the previous forum can retrieve their temporary password here, (login and check your PM).

Vacuum pump suggestions plz

Migrated topic.

Carrierwave

Rising Star
Joined
May 25, 2011
Messages
109
Merits
42
I'm in the market for a vacuum pump, looking at pumps that can do 28" of vacuum. I'm going to be buchner filtering through qualantative paper, distilling under a mild vacuum, and whatever else a home chemist would do that I'm not aware of. Will 28" cut it? Thank you!

I understand that the micron rating is used for lab vacuum pumps, but that scale doesnt bear much reference to me.
 
I have used too strong a vacuum source during filtration and learned the hard way that you'll rip the filter paper. If you get a pump capable of a strong vacuum, then you will need to regulate the vacuum. Also I would suggest that you use a trap to avoid getting liquids in your pump.
 
Right, I forgot about filter paper ripping. It will have a liquid trap. Thanks for the diaphram suggestion as well.
 
I purchased a 500ml filterflask with a rubber seal and a 70mm porcelain butchner funnel for 18.95 at Local Settlements|Virtual Accounts|Global Money Transfer|PayFX|Agile FX|England.

Heres the link: http://www.agile-fx.com/servlet/the-2518/Filtration-Kit-w-fdsh--70mm/Detail

I needed a vacuum pump to complete my filtering setup so i purchased this off ebay:


As far as i know, after lots of web browsing and searching this was the best deal for a filtering setup. I have no issues with this combo and it works very well for rue extractions. Esp. HCL manskes, was able to filter almost 6g of crystals with one filter paper.
 
If you want a hand-powered vacuum pump the best you can find is from Mityvac (esp. the "silverline").
 
hand-vac, as you can imagine, is limited to filtration. if you want to do other applications,
such as vac-distillation, sublimation, and/or vac-desiccation, a diaphragm, rocking-piston, or rotary-vane pump is recommended.
if you need to do distillation or sublimation of high-boiling compounds, you'll want a rotary-vane pump capable of pulling down to the low-micron range; check the specs.. CFM is not important in this context, absolute pressure is more important.
 
Back
Top Bottom