The 100g seems to be a good amount to work with. It just depends on your container sizes and equipment. Just make sure you have the right equipment before you start. Xylene will yield less than d-limo but if xylene is all you can get then by all means use it.
Larger amounts STB had a lower yield than smaller (up to 100grams) in my experience with the same cactus material and the same procedure.
You could rehydrate the cactus with a large amount of water, basify that, and then do a sludge/solvent extraction as shown on a vid which circulates around the net. That person used 400 grams of powder.
Boiling/straining it down into a concentrated tea and basifying that, will make it easier to handle and is less prone to emulsion problems, but takes more time.
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