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Yellow solvent

Thehogg

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The solvent isn’t clear and easily separated. It’s hard to pipette off without the mud coming up. The mud is sticking to the glass too. Too little solvent?

This was a reduction from 3 to 1 liters.
 
Simple - don't pipette straight into the precipitation dish, use a separate jug to catch any stray drops of base soup from out of the naphtha before transferring it onwards.

The solvent may be cloudy due to saturation with DMT, and a yellow colour in the naphtha is entirely normal. Pictures would be helpful towards commenting with more certainty, however.
 
Simple - don't pipette straight into the precipitation dish, use a separate jug to catch any stray drops of base soup from out of the naphtha before transferring it onwards.
Sounds familiar 😉

The solvent isn’t clear and easily separated. It’s hard to pipette off without the mud coming up. The mud is sticking to the glass too. Too little solvent?

This was a reduction from 3 to 1 liters.
A lil more solvent can serve as a buffer that wouldn't hurt and can limit the amount of soup you pull. With practice you will get better at pulling without catching any soup, and nevertheless, use the method @Transform mentions above. In using that method you're leveraging the stickiness of the soup material to keep it out of the precipitation phase.

One love
 
Quick question- what do you mean by
This was a reduction from 3 to 1 liters.
?
Does this mean:
  • that you're trying a smaller extraction overall than previously;
  • that you've decide to use less water for the same amount of bark compared to last time, or
  • that you've taken a 3 litre acidic brew and simmered it down to 1 litre?
Or maybe something else?
Reducing the volume may increase the likelihood of emulsions so a more thorough rundown on exactly what you've done so far would make it far easier to troubleshoot your situation, which (tbh) on the face of it looks like "I've f*'d it up cos I don't really understand what I'm doing". The process of explaining how you got to your situation will help you to progress positively from that space.

Sounds familiar 😉
😁 And then there's the trick of including a bit of water with a pinch of sodium carbonate to wash the pull a little. By now I should have set up macros on my keyboard for this stuff.
 
Quick question- what do you mean by

?
Does this mean:
  • that you're trying a smaller extraction overall than previously;
  • that you've decide to use less water for the same amount of bark compared to last time, or
  • that you've taken a 3 litre acidic brew and simmered it down to 1 litre?
Or maybe something else?
Reducing the volume may increase the likelihood of emulsions so a more thorough rundown on exactly what you've done so far would make it far easier to troubleshoot your situation, which (tbh) on the face of it looks like "I've f*'d it up cos I don't really understand what I'm doing". The process of explaining how you got to your situation will help you to progress positively from that space.


😁 And then there's the trick of including a bit of water with a pinch of sodium carbonate to wash the pull a little. By now I should have set up macros on my keyboard for this stuff.
Boiled down 3 liters. It was on accident. But I went with it.
 
Quick question- what do you mean by

?
Does this mean:
  • that you're trying a smaller extraction overall than previously;
  • that you've decide to use less water for the same amount of bark compared to last time, or
  • that you've taken a 3 litre acidic brew and simmered it down to 1 litre?
Or maybe something else?
Reducing the volume may increase the likelihood of emulsions so a more thorough rundown on exactly what you've done so far would make it far easier to troubleshoot your situation, which (tbh) on the face of it looks like "I've f*'d it up cos I don't really understand what I'm doing". The process of explaining how you got to your situation will help you to progress positively from that space.


😁 And then there's the trick of including a bit of water with a pinch of sodium carbonate to wash the pull a little. By now I should have set up macros on my keyboard for this stuff.
I put a little salt in it thinking it was emulsified. Didn’t make much difference
 
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