I'm also trying my first freeze precipitiation... after doing jorkests tek and getting a pretty good yield I decided to split the basified mix (dmt+fumaric acid+sodium carbonate) into two; the first I dissolved in acetone as per the tek (got about 1.2g jungle spice from that
), and the 2nd I dissolved in some warm Naptha, as Warrensaged described: I repeated 3 times, decanting each time, filtered the combined naptha, left out for a couple hours, then put in the fridge for about 12 hrs, then into the freezer where it has been for a little over 24 hrs .. when I checked this morning, there was not a lot going on.. I thought I could see some cloudy white formations but not sure.. I had moved it from a little glass dish to a jar last night, and I swear I can see some tiny crystals left on the glass dish, but they are really tiny.
I wonder, smokeydaze if you are right - maybe I need to evaporate the naptha off a bit to make the solution more saturated?
Maybe I'm just being impatient... gonna check again when I get home tonight. Perhaps my freezer is not cold enough??
I must say the smell and feel of naptha is so different to limonene! It feels kinda dirty.. my friend said it makes the place smell of mothballs! But I'm really curious to try the pure stuff, as some say it makes for a more immersive/interactive journey than the full jurema "jungle" extraction.